2,2’-二甲氧基联苯合成路线 （共 133 条）
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride; water in tetrahydrofuran; toluene T=100°C; 15 h; Inert atmosphere;
参考文献
Pitteloud, Jean-Philippe; Zhang, Zun-Ting; Liang, Yong; Cabrera, Laura; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8199 - 8212
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride; water in tetrahydrofuran; toluene T=100°C; 2 h; Inert atmosphere;
参考文献
Pitteloud, Jean-Philippe; Zhang, Zun-Ting; Liang, Yong; Cabrera, Laura; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8199 - 8212
反应条件
in acetonitrile T=0 - 50°C; Inert atmosphere; TemperatureReagent/catalyst;
参考文献
Qian, Xin; Yu, Zailu; Auffrant, Audrey; Gosmini, Corinne
Chemistry - A European Journal, 2013 , vol. 19, # 20 p. 6225 - 6229
反应条件
bis(acetylacetonate)nickel(II) in tetrahydrofuran T=20°C; 20 h; Title compound not separated from byproducts;
参考文献
Clayden, Jonathan; Julia, Marc
Journal of the Chemical Society, Chemical Communications, 1993 , # 22 p. 1682 - 1683
反应条件
bis(acetylacetonate)nickel(II) in tetrahydrofuran T=20°C; 20 h;
参考文献
Clayden, Jonathan; Julia, Marc
Journal of the Chemical Society, Chemical Communications, 1993 , # 22 p. 1682 - 1683
反应条件
1: 94 percent / sodium perborate tetrahydrate / acetic acid / 3 h / 50 °C 2: 3 percent Chromat. / Ni(PPh3)4 / tetrahydrofuran; diethyl ether / 2 h / Ambient temperature View Scheme
参考文献
Clayden, Jonathan; Cooney, J. Jonathan A.; Julia, Marc
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 1 p. 7 - 14
反应条件
CoCl2 in acetonitrile T=80°C; other acid chlorides; also with benzene, toluene, thioanisole, p-methylanisole; effect of added 2,6-di-t-butyl-4-methylphenol; Product distributionMechanism;
参考文献
Iqbal, Javed; Khan, M. A.; Nayyar, Naresh K.
Tetrahedron Letters, 1991 , vol. 32, # 38 p. 5179 - 5182
反应条件
1: 94 percent / NaBO3, AcOH 2: 24 percent Chromat. / nickel(II) acetyloacetonate, C6H5MgBr / tetrahydrofuran / 20 h / 20 °C View Scheme
参考文献
Clayden, Jonathan; Julia, Marc
Journal of the Chemical Society, Chemical Communications, 1993 , # 22 p. 1682 - 1683
反应条件
palladium diacetate; Tl(OCOCF3)3 T=60 - 70°C; selectivity in the oxidative coupling; Product distribution;
参考文献
Deiko, S. A.; Ryabov, A. D.; Yatsimirskii, A. K.; Berezin, I. B.
Doklady Chemistry, 1982 , vol. 266, p. 356 - 359
Dokl. Akad. Nauk SSSR Ser. Khim., 1982 , vol. 266, # 4 p. 874 - 878
反应条件
[2,2']bipyridinyl; potassium iodide; NiBr2bipy Ambient temperatureelectrochemical coupling; Yields of byproduct given;
参考文献
Meyer, Gilbert; Rollin, Yolande; Perichon, Jacques
Journal of Organometallic Chemistry, 1987 , vol. 333, p. 263 - 268
