2,2’-二甲氧基联苯合成路线 （共 133 条）
反应条件
aluminium trichloride in ethanethiol 0.5 h; Ambient temperature;
参考文献
Node, Manabu; Nishide, Kiyoharu; Fuji, Kaoru; Fujita, Eiichi
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4275 - 4277
反应条件
1: 80 percent / H2SO4; dimethyldioxirane; NaBr / acetone 2: 60 percent / sodium methylate; CuBr / dimethylformamide; H2O / 2 h / Heating 3: 80 percent / NaBr; oxone / acetone; H2O View Scheme
参考文献
Bovicelli, Paolo; Antonioletti, Roberto; Onori, Antonella; Delogu, Giovanna; Fabbri, Davide; Dettori, Maria Antonietta
Tetrahedron, 2006 , vol. 62, # 4 p. 635 - 639
反应条件
1: aqueous HNO3 2: aqueous HBr; glacial acetic acid; acetic acid anhydride 3: concentrated sulfuric acid 4: sodium carbonate / 200 °C 5: aqueous hydrochloric acid; tin (II)-chloride View Scheme
参考文献
Yamashiro
Nippon Kagaku Kaishi, 1938 , vol. 59, p. 186,190
Chem.Abstr., 1938 , p. 9084
反应条件
1: 80 percent / H2SO4; dimethyldioxirane; NaBr / acetone 2: 60 percent / sodium methylate; CuBr / dimethylformamide; H2O / 2 h / Heating 3: 90 percent / cerium ammonium nitrate / acetonitrile; H2O / 0.5 h / cooling View Scheme
参考文献
Bovicelli, Paolo; Antonioletti, Roberto; Onori, Antonella; Delogu, Giovanna; Fabbri, Davide; Dettori, Maria Antonietta
Tetrahedron, 2006 , vol. 62, # 4 p. 635 - 639
参考文献
Justus Liebigs Annalen der Chemie, , vol. 332, p. 62
反应条件
1: bromine 2: tetrahydrofuran 3: thiourea; AlCl3, aluminium chloride / 1,2-dichloro-ethane / 50 °C View Scheme
反应条件
1: dimethoxy-biphenyl With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane T=0 - 40°C; 17 h; 2: methyl iodide in diethyl ether; hexane T=0°C; 1.5 h; Further stages.;
参考文献
Green, Stuart; Nelson, Adam; Warriner, Stuart; Whittaker, Benjamin
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 24 p. 4403 - 4408
反应条件
diethyl ether anschliessendes Behandeln mit Dimethylsulfat;
参考文献
Gilman; Swiss; Cheney
Journal of the American Chemical Society, 1940 , vol. 62, p. 1963,1965
参考文献
Gilman; Swiss; Cheney
Journal of the American Chemical Society, 1940 , vol. 62, p. 1963,1965
反应条件
1: concentrated sulfuric acid / <0 2: hydrobromic acid; glacial acetic acid View Scheme
参考文献
Raudnitz
Chemische Berichte, 1927 , vol. 60, p. 742
Chemische Berichte, 1928 , vol. 61, p. 246
