反应条件
1: 1.) LiN(i-Pr)2 / 1.) HMPTA, THF, -75 deg C, 1 h, 2.) HMPTA, THF, 0.5 h 2: 1.) lithium bistrimethylsilylamide / 1.) HMPTA, THF, from -75 to -70 deg C, 1.5 h, 2.) HMPTA, THF, from -75 to -70 deg C, 1 h 3: 95 percent / diisobutylaluminium hydride / hexane / 1 h / -75 °C 4: 100 percent / Amberlite IRA-400 / methanol / 24 h / Ambient temperature 5: 97 percent / H2 / Lindlar's catalyst / hexane View Scheme
参考文献
Lis, L. G.; Zheldakova, T. A.; Pap, A. A.; Lakhvich, F. A.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 8.1 p. 1452 - 1455
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 8 p. 1678 - 1683
