1H-BENZIMIDAZOLE,1-BUTYL-(9CI)合成路线 （共 12 条）
反应条件
potassium hydroxide; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=20°C; 4 h;
参考文献
Le, Zhang-Gao; Chen, Zhen-Chu; Hu, Yi; Zheng, Qin-Guo
Synthesis, 2004 , # 2 p. 208 - 212
反应条件
1: 1H-benzo[d]imidazole With sodium hydride in tetrahydrofuran T=60°C; 1 h; 2: 1-iodo-butane in tetrahydrofuran T=60°C; 48 h; Further stages.;
参考文献
Liu, Qing-Xiang; Yin, Li-Na; Feng, Jin-Cheng
Journal of Organometallic Chemistry, 2007 , vol. 692, # 17 p. 3655 - 3663
反应条件
1-methoxy-4-chlorobenzene; copper(ll) bromide T=145°C; 15 h;
参考文献
Lee, Hyung-Geun; Won, Ju-Eun; Kim, Min-Jung; Park, Song-Eun; Jung, Kwang-Ju; Bo, Ram Kim; Lee, Sang-Gyeong; Yoon, Yong-Jin
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5675 - 5678
反应条件
copper(ll) bromide T=145°C; 24 h;
参考文献
Lee, Hyung-Geun; Won, Ju-Eun; Kim, Min-Jung; Park, Song-Eun; Jung, Kwang-Ju; Bo, Ram Kim; Lee, Sang-Gyeong; Yoon, Yong-Jin
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5675 - 5678
反应条件
1: 1H-benzo[d]imidazole With potassium hydroxide in dimethyl sulfoxide T=20°C; 0.5 h; 2: n-butyl chloride in dimethyl sulfoxide T=20°C; 2 h;
参考文献
Haque, Rosenani A.; Iqbal, Muhammad Adnan
Asian Journal of Chemistry, 2012 , vol. 24, # 6 p. 2625 - 2628
反应条件
copper(ll) bromide T=145°C; 24 h;
参考文献
Lee, Hyung-Geun; Won, Ju-Eun; Kim, Min-Jung; Park, Song-Eun; Jung, Kwang-Ju; Bo, Ram Kim; Lee, Sang-Gyeong; Yoon, Yong-Jin
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5675 - 5678
反应条件
1: sodium hydroxide / tetrahydrofuran / 16 h / 65 °C / |Reflux 2: tetrahydrofuran / 65 °C View Scheme
参考文献
Shannon, Matthew S.; Hindman, Michelle S.; Danielsen, Scott P.O.; Tedstone, Jason M.; Gilmore, Ricky D.; Bara, Jason E.
Science China Chemistry, 2012 , vol. 55, # 8 p. 1638 - 1647
反应条件
in tetrahydrofuran T=65°C;
参考文献
Shannon, Matthew S.; Hindman, Michelle S.; Danielsen, Scott P.O.; Tedstone, Jason M.; Gilmore, Ricky D.; Bara, Jason E.
Science China Chemistry, 2012 , vol. 55, # 8 p. 1638 - 1647
反应条件
potassium hydroxide; sodium tetrahydroborate; bis(benzonitrile)palladium(II) dichloride; dibutylamine; 3-chloro-benzenecarboperoxoic acid 1.) THF; Yield givenMultistep reaction;
参考文献
Seipelt, Christa; Lopez, Pilar; Kirschgen, Thomas; Doelle, Andreas; Zeidler, Manfred D.; Fonseca, Isabel; Cano, Felix H.; Ballesteros, Paloma
Tetrahedron Letters, 1999 , vol. 40, # 9 p. 1739 - 1742
反应条件
cyclohexa-1,4-diene in benzene-d6 T=125°C; Bergman cycloaromatization; Kinetics; Further Variations:Temperatures;
参考文献
Zhao, Zhengrong; Peng, Yunshan; Dalley, N. Kent; Cannon, John F.; Peterson, Matt A.
Tetrahedron Letters, 2004 , vol. 45, # 18 p. 3621 - 3624
