2,4,6-三苯基三嗪合成路线 （共 216 条）
反应条件
ammonium hydroxide; Fremy’s salt in pyridine 192 h; Ambient temperature;
参考文献
Llobera, A.; Saa, J. M.; Peralta, A.
Synthesis, 1985 , # 1 p. 95 - 98
反应条件
sodium hydride in tetrahydrofuran 7 h; Heating;
参考文献
Ogonor
Tetrahedron, 1981 , vol. 37, # 16 p. 2909 - 2910
反应条件
magnesium in diethylene glycol dimethyl ether Heatingovernight;
参考文献
Burns, Timothy P.; Rieke, Reuben D.
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3674 - 3680
反应条件
LiCrH4*2LiCl*2THF in tetrahydrofuran T=25°C; 12 h;
参考文献
Eisch, John J.; Shi, Xian; Alila, Joseph R.; Thiele, Sven
Chemische Berichte, 1997 , vol. 130, # 9 p. 1175 - 1187
反应条件
samarium diiodide T=80°C; 24 h;
参考文献
Xu, Fan; Sun, Jianhua; Shen, Qi
Tetrahedron Letters, 2002 , vol. 43, # 10 p. 1867 - 1869
反应条件
KCN in benzonitrile refluxing for 12 h (N2); evapn., extn. with Et2O, chromy on Florisil and recrystn. from CH2Cl2-EtOH;
参考文献
Johnson, David K.; Rukachaisirikul, Thitima; Sun, Yan; Taylor, Nicholas J.; Canty, Allan J.; Carty, Arthur J.
Inorganic Chemistry, 1993 , vol. 32, p. 5544 - 5552
反应条件
1: 1,2,3,4-tetrapropyl-1,4-diiodo-1,3-diene With tert.-butyl lithium in diethyl ether; pentane T=-78°C; 1 h; Inert atmosphere; 2: With N,N,N',N',N'',N''-hexamethylphosphoric triamide in diethyl ether; pentane T=20°C; 0.5 h; Inert atmosphere; 3: benzonitrile in diethyl ether; pentane T=20°C; 3 h; Inert atmosphere;
参考文献
Yu, Nan; Wang, Congyang; Zhao, Fei; Liu, Lantao; Zhang, Wen-Xiong; Xi, Zhenfeng
Chemistry - A European Journal, 2008 , vol. 14, # 18 p. 5670 - 5679
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform 2 h; Reflux;
参考文献
Brough, Peter; Gambarelli, Serge; Jacquot, Jean-Francois; Grand, Andre; Pecaut, Jacques; Rey, Paul
Chemistry - A European Journal, 2011 , vol. 17, # 40 p. 11250 - 11257
反应条件
samarium diiodide T=80°C; 24 h;
参考文献
Xu, Fan; Sun, Jianhua; Shen, Qi
Tetrahedron Letters, 2002 , vol. 43, # 10 p. 1867 - 1869
反应条件
1: iodine; liquid ammonia / -39 °C 2: iodine; ammonia View Scheme
参考文献
Strain
Journal of the American Chemical Society, 1927 , vol. 49, p. 1568
