2-乙酰氨基-5-甲基吡啶合成路线 (共 14 条)
反应条件
[Pd(dippf)Cl2]; triethylamine in acetonitrile T=150°C; 1 h; Microwave irradiation; chemoselective reaction;
参考文献
Fuentes, Jose A.; Clarke, Matthew L.
Synlett, 2008 , # 17 p. 2579 - 2582
参考文献
Frimannsson, Daniel O.; McCabe, Thomas; Schmitt, Wolfgang; Lawler, Mark; Gunnlaugsson, Thorfinnur
Supramolecular Chemistry, 2010 , vol. 22, # 9 p. 483 - 490
反应条件
water; fluorine T=-40 - 0°C; 2 h;
参考文献
Kiselyov; Strekowski
Synthetic Communications, 1994 , vol. 24, # 16 p. 2387 - 2392
反应条件
water; fluorine; acetonitrile T=-40 - 0°C; 2 h;
参考文献
Kiselyov; Strekowski
Synthetic Communications, 1994 , vol. 24, # 16 p. 2387 - 2392
反应条件
sodium tris(acetoxy)borohydride T=-40 - 0°C; 7 h; Further byproducts given;
参考文献
Kiselyov, Alexander S.
Tetrahedron Letters, 2005 , vol. 46, # 26 p. 4487 - 4490
反应条件
1: aqueous KMnO4 2: aqueous NaOH View Scheme
参考文献
Ferrari
Bollettino Chimico Farmaceutico, 1957 , vol. 96, p. 542,543
反应条件
1: aqueous KMnO4 2: methanol; HCl View Scheme
参考文献
Ferrari
Bollettino Chimico Farmaceutico, 1957 , vol. 96, p. 542,543
反应条件
1: aqueous KMnO4 2: methanol; HCl 3: acetic acid 4: concentrated aqueous NH3 5: concentrated aqueous NH3 / 130 °C View Scheme
参考文献
Ferrari
Bollettino Chimico Farmaceutico, 1957 , vol. 96, p. 542,543
反应条件
1: acetic acid / Erwaermen des Reaktionsprodukts mit wss. NaOH 2: concentrated sulfuric acid; aqueous hydrogen peroxide; sulfur trioxide View Scheme
参考文献
Brown
Journal of the American Chemical Society, 1957 , vol. 79, p. 3565
反应条件
1: aqueous KMnO4 2: methanol; HCl 3: acetic acid View Scheme
参考文献
Ferrari
Bollettino Chimico Farmaceutico, 1957 , vol. 96, p. 542,543