1-苯基-2-丁烯-1-酮合成路线 （共 117 条）
参考文献
Kohler
American Chemical Journal, 1909 , vol. 42, p. 393
反应条件
1: 60 percent / CH3ONa / methanol / 5 h / Ambient temperature 2: 20 percent / phenyl phosphorodiamidate / 200 °C View Scheme
参考文献
Lassalvy, Christiane; Petrus, Clement; Petrus, Francoise
Gazzetta Chimica Italiana, 1981 , vol. 111, # 7/8 p. 273 - 278
反应条件
C57H55N; dihydrogen peroxide in water; toluene T=20°C; 14 h; optical yield given as percent eeenantioselective reaction;
参考文献
Mako, Attila; Rapi, Zsolt; Keglevich, Gyoergy; Szoellsy, Aron; Drahos, Laszlo; Hegeds, Laszlo; Bako, Peter
Tetrahedron Asymmetry, 2010 , vol. 21, # 8 p. 919 - 925
反应条件
potassium cyanide; ethanol; acetic acid Erhitzen des Reaktionsprodukts mit wss. NaOH;
参考文献
Ramirez; Rubin
Journal of the American Chemical Society, 1955 , vol. 77, p. 3768,3772
反应条件
diethyl ether; bromine
nachfolgend Einw. von Piperidin und Kochen des Reaktionsprodukts mit Schwefelsaeure;
参考文献
Dufraisse; Moureu
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1927 , vol. 184, p. 99
Bulletin de la Societe Chimique de France, 1927 , vol. <4>41, p. 1375
反应条件
N,N-bis(perfluoromethanesulfonyl)squaramide in acetonitrile
T=20°C; Mukaiyama Michael reaction; 2 h;
参考文献
Cheon, Cheol Hong; Yamamoto, Hisashi
Tetrahedron, 2010 , vol. 66, # 24 p. 4257 - 4264
反应条件
1.1: Grubb's 2nd generation catalyst / dichloromethane / 12 h / Inert atmosphere; Reflux
2.1: tributylphosphine / tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
View Scheme
参考文献
Cran, John W.; Krafft, Marie E.; Seibert, Kimberly A.; Haxell, Thomas F.N.; Wright, James A.; Hirosawa, Chitaru; Abboud, Khalil A.
Tetrahedron, 2011 , vol. 67, # 51 p. 9922 - 9943
反应条件
ethanol; acetic acid
参考文献
Kohler
American Chemical Journal, 1909 , vol. 42, p. 393
反应条件
1.1: Grubb's 2nd generation catalyst / dichloromethane / 12 h / Inert atmosphere; Reflux
2.1: tributylphosphine / tert-butyl alcohol / Inert atmosphere
2.2: Inert atmosphere
View Scheme
参考文献
Cran, John W.; Krafft, Marie E.; Seibert, Kimberly A.; Haxell, Thomas F.N.; Wright, James A.; Hirosawa, Chitaru; Abboud, Khalil A.
Tetrahedron, 2011 , vol. 67, # 51 p. 9922 - 9943
反应条件
1: anschliessende Hydrolyse
View Scheme
参考文献
Barat
Journal of the Indian Chemical Society, 1931 , vol. 8, p. 704,707
Chem. Zentralbl., 1932 , vol. 103, # I p. 526
