3-碘-2-甲基-2H-吲唑合成路线 （共 4 条）
参考文献
Quanticel Pharmaceuticals, Inc.; Kanouni, Toufike; Stafford, Jeffrey Alan; Veal, James Marvin; Wallace, Michael Brennen
Patent: US2014/171432 A1, 2014 ;
Location in patent: Page/Page column ;
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran; hexane
T=0 - 5°C;
2: With iodine in tetrahydrofuran; hexane
T=-78°C; 2 h;
参考文献
Bunnell, Aaron; O'Yang, Counde; Petrica, Andra; Soth, Michael J.
Synthetic Communications, 2006 , vol. 36, # 3 p. 285 - 293
反应条件
1: NaOH-solution; iodine
2: sodium methylate solution
View Scheme
参考文献
v. Auwers; Lohr
Journal fuer Praktische Chemie (Leipzig), 1924 , vol. <2> 108, p. 314
参考文献
v. Auwers; Lohr
Journal fuer Praktische Chemie (Leipzig), 1924 , vol. <2> 108, p. 314
