反式-2-甲基-2-丁烯醛合成路线 (共 86 条)
参考文献
BASF Aktiengesellschaft
Patent: US4618704 A1, 1986 ;
参考文献
BASF Aktiengesellschaft
Patent: US4677230 A1, 1987 ;
反应条件
aluminium trichloride in dichloromethane T=-78°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Niestroj, Michael; Neumann, Wilhelm P.
Chemische Berichte, 1996 , vol. 129, # 1 p. 45 - 51
反应条件
aluminium trichloride in dichloromethane T=-78°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Niestroj, Michael; Neumann, Wilhelm P.
Chemische Berichte, 1996 , vol. 129, # 1 p. 45 - 51
反应条件
NHep4(1+)*I(1-); tributyl tin (1+); iodide in para-xylene T=119°C; 2 h; Heating / reflux;
参考文献
Eastman Chemical Company
Patent: US6342614 B1, 2002 ;
Location in patent: Example 330 ;
反应条件
1: aqueous phosphoric acid; hydroquinone 2: toluene-4-sulfonic acid / 180 °C View Scheme
参考文献
Nasarow et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 3683,3686;engl.Ausg.S.3641,3644
参考文献
Green; Hickinbottom
Journal of the Chemical Society, 1957 , p. 3270,3272
参考文献
Oroshnik; Mallory
Journal of the American Chemical Society, 1950 , vol. 72, p. 4608,4611
反应条件
T=560°C; P=170 Torr;
参考文献
Doeuvre
Bulletin de la Societe Chimique de France, 1934 , vol. <5> 1, p. 198,201
参考文献
Grignard; Abelmann
Bulletin de la Societe Chimique de France, 1910 , vol. <4>7, p. 639