1,3-苯并二氧戊环-5-基(1-苯并呋喃-2-基)甲酮合成路线 (共 2 条)
反应条件
1: 2-methyl-benzyl alcohol With potassium carbonate in acetone
T=20°C; 0.25 h;
2: 1-(1,3-benzodioxol-5-yl)-2-bromoethanone in acetone
4 h; Heating;
参考文献
Azevedo, Mariangela S.; Alves, Glaucia B. C.; Cardoso, Jari N.; Lopes, Rosangela S. C.; Lopes, Claudio C.
Synthesis, 2004 , # 8 p. 1262 - 1268
反应条件
1.1: 79 percent / CuBr2 / ethyl acetate; CHCl3 / Heating
2.1: K2CO3 / acetone / 0.25 h / 20 °C
2.2: 90 percent / acetone / 4 h / Heating
View Scheme
参考文献
Azevedo, Mariangela S.; Alves, Glaucia B. C.; Cardoso, Jari N.; Lopes, Rosangela S. C.; Lopes, Claudio C.
Synthesis, 2004 , # 8 p. 1262 - 1268