5-氨基-1,3-二甲基嘧啶-2,4(1H,3H)-二酮合成路线 （共 8 条）
反应条件
1: Heating 2: nitric acid; sulfuric acid / 1 h / Heating 3: 75 percent / acetic acid; iron / 0.5 h / Heating View Scheme
参考文献
Zajac, Matthew A.; Zakrzewski, Anthony G.; Kowal, Mark G.; Narayan, Saraswathi
Synthetic Communications, 2003 , vol. 33, # 19 p. 3291 - 3297
参考文献
Pfleiderer; Liedek
Justus Liebigs Annalen der Chemie, 1958 , vol. 612, p. 184
反应条件
1: Heating 2: nitric acid; sulfuric acid / 1 h / Heating 3: 75 percent / acetic acid; iron / 0.5 h / Heating 4: 95 percent / sodium hydride / dimethylsulfoxide / 0.75 h View Scheme
参考文献
Zajac, Matthew A.; Zakrzewski, Anthony G.; Kowal, Mark G.; Narayan, Saraswathi
Synthetic Communications, 2003 , vol. 33, # 19 p. 3291 - 3297
反应条件
hydrogenchloride; iron in tetrahydrofuran; water
0.5 h; Heating;
参考文献
Zajac, Matthew A.; Zakrzewski, Anthony G.; Kowal, Mark G.; Narayan, Saraswathi
Synthetic Communications, 2003 , vol. 33, # 19 p. 3291 - 3297
反应条件
1: 64 percent / nitric acid; sulfuric acid / 0.5 h / 20 °C
2: 70 percent / iron; hydrochloric acid / tetrahydrofuran; H2O / 0.5 h / Heating
View Scheme
参考文献
Zajac, Matthew A.; Zakrzewski, Anthony G.; Kowal, Mark G.; Narayan, Saraswathi
Synthetic Communications, 2003 , vol. 33, # 19 p. 3291 - 3297
反应条件
diethylamine
T=50°C; 20 h; Et2NH with a 90-molar excess;
参考文献
Shorshnev, S.V.; Esipov, S.E.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 2 p. 231
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 2 p. 274 - 275
参考文献
Shorshnev, S. V.; Esipov, S. E.; Kuz'menko, V. V.; Gulevskaya, A. V.; Pozharskii, A. F.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 11 p. 1289 - 1301
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 11 p. 1545 - 1558
参考文献
Kitade, Yukio; Hirota, Kosaku; Maki, Yoshifumi
Journal of Chemical Research, Miniprint, 1993 , # 1 p. 101 - 112
