4-羟基-3-甲氧基苄醇合成路线 (共 134 条)
反应条件
potassium carbonate in ethanol
参考文献
Andresen; Davis; Long
Journal of Pharmaceutical Sciences, 1979 , vol. 68, # 3 p. 283 - 288
反应条件
1: 52.6 percent / 0.1 N KOH, 0.05 N LiClO4 / acetonitrile; H2O / 0 °C / anodic oxidation at Pt electrode 2: 37.6 percent / 0.1 N KOH, 0.05 N LiClO4 / acetonitrile; H2O / 0 °C / cathodic reduction at Pt electrode View Scheme
参考文献
Yanilkin, V. V.; Dudenko, L. Yu.; Babkin, V. A.; Ivanova, S. Z.; Medvedev, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 5 p. 1139 - 1145,1001 - 1006
反应条件
sulfuric acid; nitric acid; HNO2 T=25°C; Product distributionMechanism;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 10 p. 1845 - 1850
Zhurnal Organicheskoi Khimii, , vol. 19, # 10 p. 2124 - 2130
参考文献
Andersen
Comment. phys. math. Helsingfors, 1956 , vol. 19, # 1 p. 23
反应条件
oxygen in toluene T=80°C; 24 h;
参考文献
Carrillo, Adela I.; Schmidt, Luciana C.; Marin, M. Luisa; Scaiano, Juan C.
Catalysis Science and Technology, 2014 , vol. 4, # 2 p. 435 - 440
参考文献
Chemistry of Natural Compounds, , vol. 26, # 1 p. 54 - 59
Khimiya Prirodnykh Soedinenii, , # 1 p. 67 - 74
反应条件
in N,N-dimethyl-formamide T=130°C; 20 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 15, # 14 p. 3369 - 3373
反应条件
in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere;
参考文献
Journal of Natural Medicines, , vol. 64, # 3 p. 245 - 251
反应条件
Melanocarpus albomyces laccase; oxygen in 1,4-dioxane 24 h; sodium succinate buffer;
参考文献
Maarit, Lahtinen; Kristiina, Kruus; Petri, Heinonen; Jussi, Sipilae
Journal of Agricultural and Food Chemistry, 2009 , vol. 57, # 18 p. 8357 - 8365
反应条件
1: 88 percent / p-toluenesulfonic acid / 6 h / Ambient temperature 2: 1.) n-BuLi / 1.) THF,hexane, RT, 2.) from -40 deg C to 0 deg C 3: 63 percent / aq. HCl / tetrahydrofuran 4: 89 percent / PO4HNa2/PO4H2Na, Fremy's salt View Scheme
参考文献
Saa, Jose M.; Llobera, Antonia; Garcia-Raso, Angel; Costa, Antonio; Deya, Pedro M.
Journal of Organic Chemistry, 1988 , vol. 53, # 18 p. 4263 - 4273