4'-羟基-3'-甲氧基苯乙酮合成路线 （共 147 条）
反应条件
ytterbium(III) triflate in carbon disulfide Friedel-Crafts reaction; 6 h; Heating;
参考文献
Su, Weike; Jin, Can
Synthetic Communications, 2004 , vol. 34, # 22 p. 4199 - 4205
反应条件
Ru(H)2(CO)(PPh3)(xantphos) in deuterated toluene T=135°C; P=760.051 Torr; 20 h; Inert atmosphere;
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
反应条件
RuH2(CO)(PPh3)3; hydrogen; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in deuterated toluene T=135°C; P=760.051 Torr; 20 h;
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
反应条件
1: With N-iodo-succinimide; N-hexadecyl-N,N,N-trimethylammonium bromide in 1,4-dioxane; water T=115°C; 0.25 h; Microwave irradiation; 2: With dipyridinium dichromate; acetic acid in 1,4-dioxane; water T=115°C; 0.25 h; Microwave irradiation;
参考文献
Sharma, Naina; Sharma, Abhishek; Kumar, Rakesh; Shard, Amit; Sinha, Arun K.
European Journal of Organic Chemistry, 2010 , # 31 p. 6025 - 6032
反应条件
1: DBU / dioxane / 12 h / 0 - 20 °C 2: TFA / 4 h / 0 °C 3: H2O / UV-irradiation View Scheme
参考文献
Conrad II, Peter G.; Givens, Richard S.; Weber, Joerg F. W.; Kandler, Karl
Organic Letters, 2000 , vol. 2, # 11 p. 1545 - 1547
反应条件
1: Ru(H)2(CO)(PPh3)(xantphos) / deuterated toluene / 20 h / 135 °C / 760.05 Torr / |Inert atmosphere 2: RuH2(CO)(PPh3)3; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; hydrogen / deuterated toluene / 20 h / 135 °C / 760.05 Torr View Scheme
参考文献
Galkin, Maxim V.; Sawadjoon, Supaporn; Rohde, Volker; Dawange, Monali; Samec, Joseph S. M.
ChemCatChem, 2014 , vol. 6, # 1 p. 179 - 184
参考文献
Adler; Hernestam
Acta Chemica Scandinavica (1947-1973), 1955 , vol. 9, p. 319,332
反应条件
oxygen; rose bengal in acetonitrile T=13°C; Irradiation;
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 58 percent / i-Pr2NEt 2: K2CO3 / dimethylformamide 3: HCl / methanol View Scheme
参考文献
Tsuda, Hideyuki; Ishitani, Youichi; Takemura, Yoshiyuki; Suzuki, Yoshiaki; Kato, Tadahiro
Heterocycles, 1997 , vol. 44, # 1 p. 139 - 142
反应条件
1: K2CO3 / dimethylformamide 2: HCl / methanol View Scheme
参考文献
Tsuda, Hideyuki; Ishitani, Youichi; Takemura, Yoshiyuki; Suzuki, Yoshiaki; Kato, Tadahiro
Heterocycles, 1997 , vol. 44, # 1 p. 139 - 142
