4'-羟基-3'-甲氧基苯乙酮合成路线 （共 147 条）
反应条件
1: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C 2: RuH2(CO)(PPh3)3; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; hydrogen / deuterated toluene / 20 h / 135 °C / 760.05 Torr View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
反应条件
hydrogenchloride in methanol Yield given;
参考文献
Tsuda, Hideyuki; Ishitani, Youichi; Takemura, Yoshiyuki; Suzuki, Yoshiaki; Kato, Tadahiro
Heterocycles, 1997 , vol. 44, # 1 p. 139 - 142
反应条件
1: TFA / 4 h / 0 °C 2: H2O / UV-irradiation View Scheme
参考文献
Conrad II, Peter G.; Givens, Richard S.; Weber, Joerg F. W.; Kandler, Karl
Organic Letters, 2000 , vol. 2, # 11 p. 1545 - 1547
反应条件
1: 95.3 percent / TFA / 4 h / 0 °C 2: H2O / UV-irradiation View Scheme
参考文献
Conrad II, Peter G.; Givens, Richard S.; Weber, Joerg F. W.; Kandler, Karl
Organic Letters, 2000 , vol. 2, # 11 p. 1545 - 1547
反应条件
1: potassium carbonate / acetone / 16 h / 20 °C 2: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C 3: RuH2(CO)(PPh3)3; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; hydrogen / deuterated toluene / 20 h / 135 °C / 760.05 Torr View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
反应条件
1: diethyl ether / 1 h / Heating 2: DDQ / benzene / 4 h View Scheme
参考文献
Suri, O. P.; Bindra, R. S.; Satti, N. K.; Khajuria, R. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 587 - 588
反应条件
1: potassium carbonate / acetone / 16 h / 20 °C 2: sodium hydroxide; sodium tetrahydroborate / tetrahydrofuran; water / 16 h / 20 °C 3: Ru(H)2(CO)(PPh3)(xantphos) / deuterated toluene / 20 h / 135 °C / 760.05 Torr / |Inert atmosphere View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
反应条件
water Hydrolysis; reduction; rearrangement; UV-irradiation;
参考文献
Conrad II, Peter G.; Givens, Richard S.; Weber, Joerg F. W.; Kandler, Karl
Organic Letters, 2000 , vol. 2, # 11 p. 1545 - 1547
反应条件
sodium hydroxide; nickel T=25°C; Catalytic hydrogenation; Electrochemical reaction; Product distribution; Further Variations:Temperaturesother substrates, other current densities;
参考文献
Cyr, Andre; Chiltz, Florence; Jeanson, Paul; Martel, Anna; Brossard, Louis; Lessard, Jean; Menard, Hugues
Canadian Journal of Chemistry, 2000 , vol. 78, # 3 p. 307 - 315
反应条件
potassium permanganate
参考文献
Tiemann; Nagai
Chemische Berichte, 1877 , vol. 10, p. 202
Full Text Show Details
Tiemann
Chemische Berichte, 1891 , vol. 24, p. 2856
Chemische Berichte, 1876 , vol. 9, p. 419
