4'-羟基-3'-甲氧基苯乙酮合成路线 (共 147 条)
反应条件
sulfuric acid; iron; sodium iodide
参考文献
Robinson; Robinson; Todd
Journal of the Chemical Society, 1934 , p. 809
反应条件
piperidine in 1,4-dioxane T=25°C; Deacetylation; Kinetics;
参考文献
Kurzin; Platonov; Evstigneev; Maiorova
Russian Journal of General Chemistry, 1997 , vol. 67, # 9 p. 1475 - 1477
反应条件
bei der Destillation;
参考文献
Finnemore
Journal of the Chemical Society, 1908 , vol. 93, p. 1522
Full Text Show Details
Neitzel
Chemische Berichte, 1891 , vol. 24, p. 2867
反应条件
durch Ueberfuehrung in das Carbinol, Oxydation mit Kaliumdichromat und Schwefelsaeure zu 3-Methoxy-4-benzoyloxy-acetophenon und Verseifen durch Kochen mit verd.Natronlauge;
参考文献
Finnemore
Journal of the Chemical Society, 1908 , vol. 93, p. 1522
参考文献
Dann; Mylius
Justus Liebigs Annalen der Chemie, 1954 , vol. 587, p. 1,15
参考文献
Coulthard; Marshall; Pyman
Journal of the Chemical Society, 1930 , p. 280,291
Full Text Show Details
Schorygin; Bogatschewa
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 1567
Chem. Zentralbl., 1937 , vol. 108, # I p. 1931
参考文献
Coulthard; Marshall; Pyman
Journal of the Chemical Society, 1930 , p. 280,291
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 25 °C / Inert atmosphere 2: nitric acid / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
The Regents of the University of Colorado, A Body Corporate
Patent: US8343710 B1, 2013 ;
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 50 °C 2: acetic anhydride; nitric acid / 5 h / |Cooling with ice View Scheme
参考文献
Yan, Bin; Boyer, John-Christopher; Habault, Damien; Branda, Neil R.; Zhao, Yue
Journal of the American Chemical Society, 2012 , vol. 134, # 40 p. 16558 - 16561
反应条件
pyridine in tetrahydrofuran T=20°C; 3 h;
参考文献
DIGITAL BIOTECH CO., LTD
Patent: WO2008/41826 A1, 2008 ;
Location in patent: Page/Page column 17; 35-36 ;