3,5-二溴-2-羟基-6-甲基嘧啶合成路线 (共 7 条)
反应条件
N-bromosuccinmide in acetonitrile 1 h; Heating;
参考文献
Meana, Angela; Rodriguez, Justo F.; Sanz-Tejedor, M. Ascension; Garcia-Ruano, Jose L.
Synlett, 2003 , # 11 p. 1678 - 1682
反应条件
sulfuric acid; sodium nitrite Diazotization;
参考文献
Adams; Schrecker
Journal of the American Chemical Society, 1949 , vol. 71, p. 1186,1191
反应条件
1: aqueous H2SO4; bromine 2: aqueous sulfuric acid; sodium nitrite / Diazotization View Scheme
参考文献
Adams; Schrecker
Journal of the American Chemical Society, 1949 , vol. 71, p. 1186,1191
反应条件
N-bromosuccinmide in acetonitrile Title compound not separated from byproducts;
参考文献
Meana, Angela; Rodriguez, Justo F.; Sanz-Tejedor, M. Ascension; Garcia-Ruano, Jose L.
Synlett, 2003 , # 11 p. 1678 - 1682
参考文献
Adams; Schrecker
Journal of the American Chemical Society, 1949 , vol. 71, p. 1186,1191
参考文献
Willink; Wibaut
Recueil des Travaux Chimiques des Pays-Bas, 1934 , vol. 53, p. 417,420
反应条件
1: With n-butyllithium T=-90°C; 2: With water T=-90°C;
参考文献
Meana, Angela; Rodriguez, Justo F.; Sanz-Tejedor, M. Ascension; Garcia-Ruano, Jose L.
Synlett, 2003 , # 11 p. 1678 - 1682