1: ammonium carbonate / aq. ethanol / 55 - 60 °C 2: aq. NaOH / 72 h / Heating 3: aq. NaOH / dioxane / 12 h / Ambient temperature View Scheme
参考文献
Palacin, Serge; Chin, Donovan N.; Simanek, Eric E.; MacDonald, John C.; Whitesides, George M.; McBride, Mary T.; Palmore, G. Tayhas R.
Journal of the American Chemical Society, 1997 , vol. 119, # 49 p. 11807 - 11816
hydrogen; aluminum oxide; K5PV2Mo10O40 T=300°C; Catalytic hydrogenation; P=41040 Torr; 3.5 h; Further byproducts given. Title compound not separated from byproducts;