2-(3-甲氧基苯基)乙醇合成路线 (共 48 条)
反应条件
anfangs in Aether, zuletzt in Aether und Benzol bei 60grad;
参考文献
Hewett
Journal of the Chemical Society, 1936 , p. 50
Full Text Show Details
Bergmann; Weizmann
Journal of Organic Chemistry, 1939 , vol. 4, p. 266,268
反应条件
sodium tetrahydroborate in ethanol 2 h; Heating; Yield given. Yields of byproduct given;
参考文献
Ookawa, Atsuhiro; Hiratsuka, Hiroshi; Soai, Kenso
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 1813 - 1818
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Kita, Yasuyuki; Egi, Masahiro; Takada, Takeshi; Tohma, Hirofumi
Synthesis, 1999 , # 5 p. 885 - 897
反应条件
1: sulfuryl chloride / CH2Cl2 / -78 °C 2: 52 percent / lithium; 4,4'-di-tert-butylbiphenyl / tetrahydrofuran / 1 h / -40 °C View Scheme
参考文献
Gomez, Cecilia; Macia, Beatriz; Lillo, Victor J.; Yus, Miguel
Tetrahedron, 2006 , vol. 62, # 42 p. 9832 - 9839
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Cueille,G. et al.
Bulletin de la Societe Chimique de France, 1972 , p. 306 - 317
反应条件
aluminium trichloride T=0 - 5°C;
参考文献
Colonge; Rochas
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1946 , vol. 223, p. 403
Bulletin de la Societe Chimique de France, 1948 , p. 818,821
反应条件
1: aqueous NaOH / Electrolysis.anschliessende Behandlung mit Dimethylsulfat und NaOH 2: pyridine; SOCl2 / <30 3: ethanol; sodium iodide 4: sulfuric acid 5: sodium View Scheme
参考文献
Rapson; Robinson
Journal of the Chemical Society, 1935 , p. 1533,1543
反应条件
1: sulfuric acid 2: sodium View Scheme
参考文献
Rapson; Robinson
Journal of the Chemical Society, 1935 , p. 1533,1543
反应条件
1: ethanol; sodium iodide 2: sulfuric acid 3: sodium View Scheme
参考文献
Rapson; Robinson
Journal of the Chemical Society, 1935 , p. 1533,1543
反应条件
bei Siedetemperatur; Einleiten von Aethylenoxyd in das auf 5grad abgekuehlte Reaktionsgemisch;
参考文献
Bachmann; Thomas
Journal of the American Chemical Society, 1942 , vol. 64, p. 94,95