1-氯-3-甲基-2-丁烯合成路线 (共 287 条)
反应条件
T=50°C; P=7500600 Torr; 72 h; Yield given. Yields of byproduct given;
参考文献
Yamamoto, Yoshinori; Maruyama, Kazuhiro; Matsumoto, Kiyoshi
Journal of the Chemical Society, Chemical Communications, 1984 , # 8 p. 548 - 549
反应条件
in water
48 h; Ambient temperature;
参考文献
Tani, Kazuhide; Yamagata, Tsuneaki; Akutagawa, Susumu; Kumobayashi, Hidenori; Taketomi, Takanao; et al.
Journal of the American Chemical Society, 1984 , vol. 106, # 18 p. 5208 - 5217
反应条件
1: diethyl ether
2: aq. NaOH
View Scheme
参考文献
Babayan,A.T. et al.
Zhurnal Organicheskoi Khimii, 1966 , vol. 2, p. 1974 - 1983,1939 - 1945
参考文献
Pudowik; Schergina
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2750,2753; engl. Ausg. S. 2789, 2791
参考文献
Edmundson,R.S.; Moran,T.A.
Journal of the Chemical Society [Section] C: Organic, 1970 , p. 1009 - 1012
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Nasarow et al.
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 611,614; engl. Ausg. S. 671, 673
反应条件
Product distributionMechanism;
参考文献
Feoktistov, V. M.; Bunina-Krivorukova, L. I.; Aleksandrova, E. K.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1977 - 1984
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 10 p. 2170 - 2178
反应条件
acetic acid
T=25°C; dann bei 50-60grad;
参考文献
Nasarow; Aserbajew
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 419,421
Chem.Abstr., 1949 , p. 114
反应条件
1: NaHCO3 / >50
2: hydrogen chloride / 0 °C
3: NaHCO3 / 50 °C
4: hydrogen chloride / 0 °C
5: glacial acetic acid / 25 °C / dann bei 50-60grad
View Scheme
参考文献
Nasarow; Aserbajew
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 419,421
Chem.Abstr., 1949 , p. 114
参考文献
Semenow et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 5472,5474
反应条件
sodium
1.) ether, 1 h, 2.) ether, reflux, 30 min; Yield given. Multistep reaction;
参考文献
Yamada, Shigetoshi; Takeshita, Toru; Tanaka, Juntaro
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 9 p. 2901 - 2902