1-氯-3-甲基-2-丁烯合成路线 （共 287 条）
参考文献
Ultee
Recueil des Travaux Chimiques des Pays-Bas, 1949 , vol. 68, p. 130
反应条件
1: 75 percent / 1.) n-BuLi / 1.) THF-hexane, -45 deg C, 40 min, 2.) -45 deg C, 40 min; -> 10 deg C 1 h 2: Li / diethyl ether; liquid ammonia / -65 °C / other reagent, solvent, temperature View Scheme
参考文献
Veselovskii, V. V.; Koptenkova, V. A.; Novikova, M. A.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 2 p. 1887 - 1891
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , vol. 9, p. 2052 - 2056
反应条件
lithium aluminium tetrahydride; silver perchlorate in tetrahydrofuran T=-50°C; 2 h;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Chemistry Letters, 1983 , p. 1877 - 1878
反应条件
lithium aluminium tetrahydride; silver perchlorate in tetrahydrofuran T=-20°C; 0.5 h;
参考文献
Chemistry Letters, , p. 1877 - 1878
反应条件
(i) Mg, THF, (ii) CuI; Multistep reaction;
参考文献
Johnston; Slessor
Canadian Journal of Chemistry, 1979 , vol. 57, # 2 p. 233 - 235
参考文献
Nasarow et al.
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 611,614; engl. Ausg. S. 671, 673
反应条件
(i) Mg, THF, (ii) CuI; Multistep reaction;
参考文献
Johnston; Slessor
Canadian Journal of Chemistry, 1979 , vol. 57, # 2 p. 233 - 235
参考文献
Nasarow et al.
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 611,614; engl. Ausg. S. 671, 673
反应条件
sodium hydrogencarbonate T=50°C;
参考文献
Nasarow; Aserbajew
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 419,421
Chem.Abstr., 1949 , p. 114
反应条件
dilithium tetrachlorocuprate in tetrahydrofuran T=0°C;
参考文献
Tetrahedron Letters, , vol. 23, # 31 p. 3115 - 3118
