1: isopropylmagnesium chloride With indium(III) chloride in tetrahydrofuran; hexane
T=-78 - 20°C;
2: carbon monoxide; 1-(iodo)-4-methylbenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane
T=60°C; 1 h;
参考文献
Lee, Sung Wook; Lee, Kooyeon; Seomoon, Dong; Kim, Sundae; Kim, Hyunseok; Kim, Hyun; Shim, Eunkyong; Lee, Miae; Lee, Seokju; Kim, Misook; Lee, Phil Ho
Journal of Organic Chemistry, 2004 , vol. 69, # 14 p. 4852 - 4855
1: With copper(I) bromide in tetrahydrofuran; 2-methyl tetrahydrofuran
T=0 - 60°C; 4 h; Inert atmosphere;
2: With water in tetrahydrofuran; 2-methyl tetrahydrofuran
T=0°C; Inert atmosphere;
3: With sulfuric acid in tetrahydrofuran; 2-methyl tetrahydrofuran
1 h; Inert atmosphereReflux;
参考文献
Monfette, Sebastien; Turner, Zoe R.; Semproni, Scott P.; Chirik, Paul J.
Journal of the American Chemical Society, 2012 , vol. 134, # 10 p. 4561 - 4564
