1: With NiII chloride hexahydrate in tetrahydrofuran; toluene
T=20°C; 1 h; Inert atmosphereSchlenk technique;
2: With water in tetrahydrofuran; toluene
Inert atmosphereSchlenk technique; stereoselective reaction;
参考文献
Xue, Fei; Zhao, Jin; Hor, T. S. Andy
Chemical Communications, 2013 , vol. 49, # 86 p. 10121 - 10123
1: n-butyllithium With anhydrous iron chloride in hexanes
T=-78°C; 3 h; Inert atmosphere;
2: diphenyl acetylene in hexanes
T=-78 - 25°C; Inert atmosphere;
3: With hydrogenchloride; water in hexanes
参考文献
Eisch, John J.; Sohn, Jane U.; Rabinowitz, Edon J.
European Journal of Organic Chemistry, 2010 , # 15 p. 2971 - 2977
