次氮基-氰基二硫基-甲烷合成路线 （共 120 条）
反应条件
in dichloromethane
T=0°C; 1.5 h;
参考文献
Tokumitsu, Takao; Hayashi, Takayuki
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1547 - 1550
反应条件
in tetrachloromethane
参考文献
Bullpitt,M.L.; Kitching,W.
Journal of Organometallic Chemistry, 1972 , vol. 34, p. 321 - 328
反应条件
in further solvent(s)
byproducts: (FCN)3; reactn. of a soln. of dirhodane in FCl2C-CClF2 with diluted F2 (F2:N2 0 1:10); cooled down to -183°C; solvent removed by condensation; mixt. condensed to aq. KOH-soln. at room temp. to remove SF4, SOF and (FCN)3; sepn. by fractionated condensation at -127°C, -140°C, -196°C;
参考文献
Loesking, Oliver; Willner, Helge
Angewandte Chemie, 1989 , vol. 101, # 9 p. 1283 - 1284
参考文献
Michalski; Wieczorkowski
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, 1957 , vol. <III> 5, p. 917,919
参考文献
Gupta; Mandal, Debprasad; Dixit, Vandana
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2002 , vol. 41, # 5 p. 970 - 972
反应条件
iodine in benzene
T=40°C; 1 h; Irradiation; Further byproducts given. Yields of byproduct given;
参考文献
Cambie, Richard C.; Rutledge, Peter S.; Strange, Gary A.; Woodgate, Paul D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 553 - 565
反应条件
iodine in benzene
18 h; Ambient temperatureother time; Product distribution;
参考文献
Cambie, Richard C.; Rutledge, Peter S.; Strange, Gary A.; Woodgate, Paul D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 553 - 565
反应条件
iodine in benzene
17.5 h; Ambient temperatureIrradiation; Further byproducts given. Yields of byproduct given;
参考文献
Cambie, Richard C.; Rutledge, Peter S.; Strange, Gary A.; Woodgate, Paul D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 553 - 565
反应条件
iodine in benzene
18 h; Irradiationother temperature; Product distribution;
参考文献
Cambie, Richard C.; Rutledge, Peter S.; Strange, Gary A.; Woodgate, Paul D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 553 - 565
反应条件
in carbon disulfide; ethanol
shaking for several hours; pptn.;
参考文献
Gmelin Handbook: Cd: SVol., 13.2, page 649 - 659
