(2,6-iPr2PhNH)5SmLi2(THF)2 in hexane T=20°C; 0.0833333 h; Schlenk techniqueInert atmosphere;

chloro-trimethyl-silane; lithium perchlorate in diethyl ether T=20°C; 0.0833333 h;

KF in dichloromethane; phosphorous acid diethyl ester

hydrogenchloride in diethyl ether; dichloromethane T=-10°C; 1 h;

1: phosphorous acid diethyl ester With [(Me3Si)2N]3La(μ-Cl)Li(THF)3 in toluene Pudovik reaction; 0.166667 h; Inert atmosphere; 2: 3-nitro-benzaldehyde in toluene T=25°C; Pudovik reaction; 0.0833333 h; Inert atmosphere;