2-氯-1-(2-萘基)乙酮合成路线 （共 17 条）
反应条件
1: benzene 2: aqueous methanolic KOH-solution 3: beim Erhitzen ueber den Schmelzpunkt 4: amalgamated zinc; concentrated hydrochloric acid; hydrogen chloride View Scheme
参考文献
Schroeter; Mueller; Huang
Chemische Berichte, 1929 , vol. 62, p. 649
参考文献
Schroeter; Mueller; Huang
Chemische Berichte, 1929 , vol. 62, p. 649
反应条件
1: benzene 2: aqueous methanolic KOH-solution 3: beim Erhitzen ueber den Schmelzpunkt View Scheme
参考文献
Schroeter; Mueller; Huang
Chemische Berichte, 1929 , vol. 62, p. 649
反应条件
N,N,N-trimethylbenzenemethanaminium dichloroiodate in methanol; 1,2-dichloro-ethane
5 h; Heating;
参考文献
Kajigaeshi, Shoji; Kakinami, Takaaki; Moriwaki, Masayuki; Fujisaki, Shizuo; Maeno, Kimihiro; Okamoto, Tsuyoshi
Synthesis, 1988 , # 7 p. 545 - 546
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(I) thiophene-2-carboxylate; trifuran-2-yl-phosphane in tetrahydrofuran
T=50°C; 18 h;
参考文献
Liebeskind; Srogl
Journal of the American Chemical Society, 2000 , vol. 122, # 45 p. 11260 - 11261
反应条件
N-chloro-succinimide; toluene-4-sulfonic acid in acetonitrile
1 h; Reflux;
参考文献
Zhu, Yan-Ping; Cai, Qun; Gao, Qing-He; Jia, Feng-Cheng; Liu, Mei-Cai; Gao, Meng; Wu, An-Xin
Tetrahedron, 2013 , vol. 69, # 31 p. 6392 - 6398
反应条件
ethylmagnesium bromide in tetrahydrofuran
T=-70 - -40°C; 2 h;
参考文献
Satoh Tsuyoshi; Mizu, Yasuhiro; Kawashima, Taku; Yamakawa, Koji
Tetrahedron, 1995 , vol. 51, # 3 p. 703 - 710
反应条件
Pd2(dba)3*CHCl3/tris(2-furyl)phosphine in tetrahydrofuran
addn. of 1.6 equiv. of C4H3SCOOCu to the reaction of ClCH2COSC6H4CH3 (1equiv.) with (C10H7)B(OH)2 (1 equiv.) in THF in presence of 1percent Pd2(dba)3*CHCl3/(tris-2-furylphosphine), holding for 18 h at 50°C;
参考文献
Liebeskind; Srogl
Journal of the American Chemical Society, 2000 , vol. 122, # 45 p. 11260 - 11261
反应条件
S4N4*SbCl5 in toluene
3 h; Heating;
参考文献
Kim, Kil-Joong; Kim, Kyongtae
Tetrahedron Letters, 1997 , vol. 38, # 24 p. 4227 - 4230
反应条件
aluminium trichloride in 1,2-dichloro-ethane
T=0°C; 0.166667 h;
参考文献
Murakami, Yasuoki; Tani, Masanobu; Tanaka, Kenjiro; Yokoyama, Yuusaku
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, p. 2023 - 2035
