2-氯-1-(2-萘基)乙酮合成路线 (共 17 条)
反应条件
in 1,2-dichloro-ethane
参考文献
Fujisawa Pharmaceutical Co., Ltd.
Patent: US5387710 A1, 1995 ;
反应条件
in diethyl ether
T=0 - 20°C;
参考文献
Happer, D. Alan R.; Hayman, Colin M.; Storer, Malina K.; Lever, Michael
Australian Journal of Chemistry, 2004 , vol. 57, # 5 p. 467 - 472
反应条件
1: 77 percent / LDA / tetrahydrofuran / 0.5 h / -65 °C
2: 63 percent / EtMgBr / tetrahydrofuran / 2 h / -70 - -40 °C
View Scheme
参考文献
Satoh Tsuyoshi; Mizu, Yasuhiro; Kawashima, Taku; Yamakawa, Koji
Tetrahedron, 1995 , vol. 51, # 3 p. 703 - 710
反应条件
aluminium trichloride; dichloromethane
T=20°C;
参考文献
Mahfouz, Nadia M.; Moharram, Ahmad M.
Pharmacy and Pharmacology Communications, 1999 , vol. 5, # 5 p. 315 - 322
参考文献
Widman
Chemische Berichte, 1918 , vol. 51, p. 911
Full Text Show Details
Morgan; Stanley
Journal of the Society of Chemical Industry, London, 1925 , vol. 44, p. 494 T
Chem. Zentralbl., 1926 , vol. 97, # I p. 927
参考文献
Morgan; Stanley
Journal of the Society of Chemical Industry, London, 1925 , vol. 44, p. 494 T
Chem. Zentralbl., 1926 , vol. 97, # I p. 927
反应条件
methanol; sodium iodide
参考文献
Rabcewicz-Zubkowski
Roczniki Chemii, vol. 9, p. 538
Chem. Zentralbl., 1929 , vol. 100, # II p. 2775