beta-甲基-alpha,alpha-二苯基哌啶-1-乙醇合成路线 (共 7 条)
反应条件
diisobutylaluminium hydride in dichloromethane; toluene
T=-70°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Moehre, H.; Kamper, Ch.
Pharmazie, 1983 , vol. 38, # 8 p. 512 - 520
反应条件
1: diethyl ether
2: diethyl ether
View Scheme
参考文献
Farbw. Hoechst
Patent: US2827460 , 1955 ;
反应条件
1: diethyl ether
2: diethyl ether
View Scheme
参考文献
Farbw. Hoechst
Patent: US2827460 , 1955 ;
参考文献
Farbw. Hoechst
Patent: US2827460 , 1955 ;
参考文献
Farbw. Hoechst
Patent: US2827460 , 1955 ;
反应条件
1: 100 percent Chromat. / HgO, Na2EDTA / ethanol; H2O / 1 h / 80 °C
2: 86 percent / dimethylsulfoxide / 13 h / Heating
View Scheme
参考文献
Moehre, H.; Kamper, Ch.
Pharmazie, 1983 , vol. 38, # 8 p. 512 - 520
反应条件
triphenylmethane tetrafluoroborate in acetonitrile
6 h; Heating; Yield given;
参考文献
Moehre, H.; Kamper, Ch.
Pharmazie, 1983 , vol. 38, # 8 p. 512 - 520