反应条件
1: 1.) lithium amide / 1.) liq. NH3/THF, -30 deg C, 1 h; 2.) liq. NH3/THF, 6 h, reflux; 3.) THF, 18 h, reflux
2: 1.) sodium hydride / 1.) mineral oil/ethane-1,2-diol, 0.5 h; 2.) mineral oil/ethane-1,2-diol, 18 h, reflux
View Scheme
参考文献
Buckle, Derek, R.; Rockell, Caroline J. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2443 - 2446
