2,3-二溴-1-丙烯合成路线 (共 153 条)
参考文献
Nelson; Wollensak
Journal of the American Chemical Society, 1958 , vol. 80, p. 6626,6628
反应条件
iron(II) sulfate in water; dimethyl sulfoxide 0.166667 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 25 p. 9609 - 9616
反应条件
in tetrahydrofuran 13 h; Ambient temperature;
参考文献
Fiandanese, V.; Marchese, G.; Naso, F.; Ronzini, L.
Synthesis, 1987 , # 11 p. 1034 - 1036
反应条件
in benzene 20 deg C, then Rt 3 h, then 60 deg C, 30 min;
参考文献
Marxer, Adrian von
Helvetica Chimica Acta, 1982 , vol. 65, # 1 p. 392 - 401
反应条件
potassium tert-butylate in dimethyl sulfoxide T=110°C; 8 h;
参考文献
Yasmin, Nasima; Ray, Jayanta K.
Synlett, 2009 , # 17 p. 2825 - 2827
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Hennings, D. David; Iwasa, Seiji; Rawal, Viresh H.
Tetrahedron Letters, 1997 , vol. 38, # 36 p. 6379 - 6382
反应条件
1: phenol With sodium hydride in tetrahydrofuran 2: 1,2-dibromo-2-propene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 16 h; Further stages.;
参考文献
Organ, Michael G.; Arvanitis, Elena A.; Dixon, Craig E.; Cooper, Jeremy T.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1288 - 1294
反应条件
1: methylmalonic acid dimethyl ester; phenol With sodium hydride in tetrahydrofuran T=20°C; 2: 1,2-dibromo-2-propene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 18 h;
参考文献
Organ, Michael G.; Arvanitis, Elena A.; Hynes, Stephen J.
Journal of Organic Chemistry, 2003 , vol. 68, # 10 p. 3918 - 3922
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 4 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Organ, Michael G.; Arvanitis, Elena A.; Hynes, Stephen J.
Tetrahedron Letters, 2002 , vol. 43, # 49 p. 8989 - 8992
反应条件
(PPh3)4 in tetrahydrofuran Ambient temperatureregioselectivity of nucleophilic attack of phenoxide-based anions on Pd-dibromo- and brompropene complexes; Product distributionMechanism;
参考文献
Organ, Michael G.; Miller, Michael
Tetrahedron Letters, 1997 , vol. 38, # 47 p. 8181 - 8184