ammonia in acetonitrile neopentylSnMe3 in CH3CN added to Fe(phen)3(PF6)3 in CH3CN at 22°C under Ar and soln. stirred for 2 h, drop water added and Fe(II) complex filtered, filtrate dried with MgSO4 and treated anhyd. NH3 and Sn product filtered;
参考文献
Rollick; Kochi
Journal of the American Chemical Society, 1982 , vol. 104, # 5 p. 1319 - 1330
hydrogen; pentacyanocobaltate(II)(3-) in water T=45°C; P=760 Torr; 10 h; <Me2C(OH)CCH>/<Co> : 1; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Funabiki, Takuzo; Yamazaki, Yasuyuki; Sato, Yoshihiro; Yoshida, Satohiro
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 12 p. 1915 - 1918