2,3-二甲基-1,3-丁二烯合成路线 （共 777 条）
反应条件
1: With carbon monoxide; {Pd([1,10]phenanthroline)2}[BF4]2; triethylamine in tetrahydrofuran T=100°C; P=7500.75 Torr; 6 h; 2: in benzene T=200°C; P=7500.75 Torr; 3 h; Further stages. Title compound not separated from byproducts.;
参考文献
Ragaini, Fabio; Cenini, Sergio; Brignoli, Daniela; Gasperini, Michela; Gallo, Emma
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 460 - 466
反应条件
carbon monoxide; {Pd([1,10]phenanthroline)2}[BF4]2; triethylamine in tetrahydrofuran T=100°C; P=7500.75 Torr; 6 h; Title compound not separated from byproducts.;
参考文献
Ragaini, Fabio; Cenini, Sergio; Brignoli, Daniela; Gasperini, Michela; Gallo, Emma
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 460 - 466
反应条件
carbon monoxide; {Pd([1,10]phenanthroline)2}[BF4]2; triethylamine in tetrahydrofuran T=100°C; P=7500.75 Torr; 6 h; Title compound not separated from byproducts.;
参考文献
Ragaini, Fabio; Cenini, Sergio; Brignoli, Daniela; Gasperini, Michela; Gallo, Emma
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 460 - 466
反应条件
1: With carbon monoxide; {Pd([1,10]phenanthroline)2}[BF4]2; triethylamine in tetrahydrofuran T=100°C; P=7500.75 Torr; 6 h; 2: in benzene T=200°C; P=7500.75 Torr; 3 h; Further stages. Title compound not separated from byproducts.;
参考文献
Ragaini, Fabio; Cenini, Sergio; Brignoli, Daniela; Gasperini, Michela; Gallo, Emma
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 460 - 466
反应条件
T=600°C; P=2.3 Torr;
参考文献
Schenk, Wolfdieter A.; Stubbe, Michael
Journal of Organometallic Chemistry, 1993 , vol. 450, # 1.2 p. C4 - C6
参考文献
Staudinger; Endle; Herold
Chemische Berichte, 1913 , vol. 46, p. 2472
反应条件
dicobalt octacarbonyl; diethyl ether; hydrogen
T=135 - 175°C; P=239040 - 286848 Torr;
参考文献
Klimova,E.I. et al.
Zhurnal Organicheskoi Khimii, 1970 , vol. 6, # 3 p. 413 - 418,411 - 416
反应条件
T=175°C; P=257428 Torr;
参考文献
Adkins; Williams
Journal of Organic Chemistry, 1952 , vol. 17, p. 980,986
反应条件
Sc(OPf)3 in hexane
T=20°C; hetero Diels-Alder reaction; 20 h;
参考文献
Hanamoto, Takeshi; Sugimoto, Yuichi; Jin, Yong Zhi; Inanaga, Junji
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 6 p. 1421 - 1426
反应条件
trifluorormethanesulfonic acid in toluene
16 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Aggarwal, Varinder K.; Vennall, Graham P.; Davey, Paul N.; Newman, Chris
Tetrahedron Letters, 1997 , vol. 38, # 14 p. 2569 - 2572
