2,3-二甲基-1,3-丁二烯合成路线 （共 777 条）
反应条件
ozone
T=-78°C; Yields of byproduct given;
参考文献
Griesbaum, Karl; Keul, Helmut; Agarwal, Sudhir; Zwick, Gerhard
Chemische Berichte, 1983 , vol. 116, # 2 p. 409 - 415
反应条件
ozone in methanol
T=-78°C; var. solvents; Product distributionMechanism;
参考文献
Griesbaum, Karl; Zwick, Garhard; Agarwal, Sudhir; Keul, Helmut; Pfeffer, Bernd; Murray, Robert W.
Journal of Organic Chemistry, 1985 , vol. 50, # 22 p. 4194 - 4199
反应条件
potassium tert-butylate in dimethyl sulfoxide
2 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Tolbert,L.M.; Siddiqui,S.
Journal of the American Chemical Society, 1984 , vol. 106, p. 5538
反应条件
1: 170 - 180 °C
2: selenium / 350 - 360 °C
View Scheme
参考文献
Alder; Rickert
Chemische Berichte, 1938 , vol. 71, p. 379,384
反应条件
hydroquinone in benzene
T=180°C; 15 h; Sealed tubeInert atmosphere;
参考文献
Geary, Laina M.; Chen, Te-Yu; Montgomery, T. Patrick; Krische, Michael J.
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 5920 - 5922
反应条件
hydrogen bromide in acetic acid
48 h;
参考文献
McCullough, John J.; MacInnis, W. Keith; Lock, Colin J. L.; Faggiani, Rommulo
Journal of the American Chemical Society, 1982 , vol. 104, # 17 p. 4644 - 4658
参考文献
Howard et al.
Journal of Research of the National Bureau of Standards (United States), 1947 , vol. 38, p. 391
Chem. Zentralbl., 1947 , vol. 118, p. 5291
反应条件
in methanol
5 h; Heating;
参考文献
Volz, Wolfgang; Voss, Juergen
Synthesis, 1990 , # 8 p. 670 - 674
反应条件
bis(1,5-cyclooctanediylboryl)monoselenide in dichloromethane; benzene
T=110°C; 18 h; Yields of byproduct given;
参考文献
Shimada, Kazuaki; Jin, Norikazu; Kawaguchi, Michiko; Dobashi, Kumiko; Nagano, Yumi; Fujimura, Manabu; Kudoh, Eiichi; Kai, Tomonari; Saito, Noboru; Masuda, Jun-Ichi; Iwaya, Masaki; Fujisawa, Hiroyuki; Aoyagi, Shigenobu; Takikawa, Yuji
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 1 p. 197 - 206
反应条件
1: C12H27Cl2PSi With sodium in n-heptane
T=90°C; 5 h;
2: 2,3-dimethyl-buta-1,3-diene in n-heptane
T=90°C; 72 h;
参考文献
Wiberg, Nils; Woerner, Angelika; Lerner, Hans-Wolfram; Karaghiosoff, Konstantin
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2002 , vol. 57, # 9 p. 1027 - 1035
