4-四氢吡喃基氧基-丁烷-1-醇合成路线 (共 25 条)
反应条件
1: PPTS / CH2Cl2 2: LiAlH4 / diethyl ether View Scheme
参考文献
Dieskau, Andre P.; Plietker, Bernd
Organic Letters, 2011 , vol. 13, # 20 p. 5544 - 5547
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Tori, Motoo; Toyoda, Naoko; Sono, Masakazu
Journal of Organic Chemistry, 1998 , vol. 63, # 2 p. 306 - 313
反应条件
chlorodimethyl(phenylthio)chloride methanaminium; triethylamine in dichloromethane T=20°C; Chlorination; 3 h;
参考文献
Gomez; Gellibert; Wagner; Mioskowski
Tetrahedron Letters, 2000 , vol. 41, # 32 p. 6049 - 6052
反应条件
erbium(III) chloride T=50°C; 0.2 h;
参考文献
Australian Journal of Chemistry, , vol. 60, # 1 p. 75 - 79
反应条件
scandium tris(trifluoromethanesulfonate) Yield given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 8 p. 2420 - 2421
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-78°C; Swern oxidation; 1 h;
参考文献
Krishna, Palakodety Radha; Srinivas, Ravula
Tetrahedron Asymmetry, 2008 , vol. 19, # 9 p. 1153 - 1160
反应条件
ammonium nitrate; Montmorillonite-K10 deprotection; 0.0416667 h; microwave irradiation;
参考文献
Meshram; Sumithra; Reddy; Ganesh; Yadav
Synthetic Communications, 1999 , vol. 29, # 16 p. 2807 - 2815
反应条件
tetrabutylammomium bromide; chlorodimethyl(phenylthio)chloride methanaminium; triethylamine in dichloromethane T=20°C; Bromination;
参考文献
Gomez; Gellibert; Wagner; Mioskowski
Tetrahedron Letters, 2000 , vol. 41, # 32 p. 6049 - 6052
反应条件
2: 82 percent / ethylenediamine / dimethylsulfoxide / 24 h / Ambient temperature View Scheme
参考文献
Naoshima; Nakamura; Munakata; Kamezawa; Tachibana
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 4 p. 1263 - 1265
参考文献
Crisostomo, Fernando R. P.; Martin, Tomas; Martin, Victor S.
Organic Letters, 2004 , vol. 6, # 4 p. 565 - 568