1,1'-(3-甲基-1-环丙烯-1,2-二基)二苯合成路线 (共 4 条)
反应条件
1,1-dimethylethylmagnesium chloride in tetrahydrofuran
1.) -78 deg C, 1 h, 2.) 25 deg C, 2 h; Title compound not separated from byproducts;
参考文献
Padwa, Albert; Goldstein, Steven I.; Rosenthal, Robert J.
Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3278 - 3285
反应条件
in tetrahydrofuran
1.) -78 deg C, 1 h, 2.) RT, 2 h;
参考文献
Padwa, Albert; Goldstein, Steven I.; Rosenthal, Robert J.
Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3278 - 3285
反应条件
water; magnesium in tetrahydrofuran
3 h; Ambient temperatureother trihalides; Product distribution;
参考文献
Ashby, E. C.; Al-Fekri, Dheya M.
Journal of Organometallic Chemistry, 1990 , vol. 390, # 3 p. 275 - 292
反应条件
aluminium trichloride in dichloromethane
T=-78 - 20°C;
参考文献
Bartmann, Ekkehard; Gompper, Rudolf
Synthetic Communications, 1987 , vol. 17, # 3 p. 263 - 270