2,3-二氯-1,4-苯醌合成路线 （共 21 条）
反应条件
1.1: 100 percent / diethyl ether / 5 h / 20 °C 2.1: 97 percent / tetrabutylammonium hydrogen sulfate / CH2Cl2; H2O / 0.03 h 3.1: 0.07 h / 165 - 170 °C / 0.5 Torr 4.1: benzene / 3 h / Heating 4.2: 63 percent / hydrochloric acid / benzene / 0.25 h / Heating 5.1: 75 percent / potassium carbonate; tris-(3,6-dioxaoctyl)-amine / dimethylsulfoxide / 3 h / 20 °C View Scheme
参考文献
Ferreira, Vitor F.; Park, Aeri; Schmitz, Francis J.; Valeriote, Fred A.
Tetrahedron, 2003 , vol. 59, # 8 p. 1349 - 1357
反应条件
chloroform durch Chlorierung;
参考文献
Oliveri-Tortorici
Gazzetta Chimica Italiana, 1897 , vol. 27 II, p. 575
参考文献
Oliveri-Tortorici
Gazzetta Chimica Italiana, 1897 , vol. 27 II, p. 575
反应条件
1: acetic acid 2: CrO3 View Scheme
参考文献
Grinew; Ermakowa; Terentjew
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 86,87
J. Gen. Chem. USSR (Engl. Transl.), 1959 , vol. 29, p. 88,89
参考文献
Chudek, John A.; Foster, Roy; Reid, Francis J.
Journal of the Chemical Society, Chemical Communications, 1983 , # 13 p. 726 - 727
参考文献
Chudek, John A.; Foster, Roy; Reid, Francis J.
Journal of the Chemical Society, Chemical Communications, 1983 , # 13 p. 726 - 727
反应条件
sodium hydroxide; acetic acid in chloroform
参考文献
Energy Conversion Devices, Inc.
Patent: US4532078 A1, 1985 ;
反应条件
sulfuric acid in acetic acid
T=60°C; 24 h;
参考文献
Pochorovski, Igor; Boudon, Corinne; Gisselbrecht, Jean-Paul; Ebert, Marc-Olivier; Schweizer, W. Bernd; Diederich, Francois
Angewandte Chemie - International Edition, 2012 , vol. 51, # 1 p. 262 - 266
反应条件
in benzene
T=25°C; 10 h;
参考文献
Oshima, Takumi; Nagai, Toshikazu
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 2507 - 2512
反应条件
in hexane; dichloromethane
-78 deg C, 1 h, then room temp., 2 h;
参考文献
Ferreira, Vitor F.; Schmitz, Francis J.
Journal of Organometallic Chemistry, 1998 , vol. 571, # 1 p. 1 - 6
