1-氯-2-甲基-2-苯基丙烷合成路线 （共 56 条）
反应条件
lithium aluminium tetrahydride; di-tert-butyl peroxide in diethyl ether 3 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 16 p. 907
反应条件
titanium(IV) isopropylate; ethylmagnesium bromide in diethyl ether Reduction; 48 h; Heating; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 7 p. 1603 - 1618
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1438,1440
反应条件
T=451.6°C; Ea, var. temp., pressure, and var. conc. of toluene inhibitor; Rate constantProduct distributionKinetics;
参考文献
Chuchani, Gabriel; Dominguez, Rosa M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 7 p. 1499 - 1502
反应条件
azoisobutyric acid dinitrle byproducts: C6H5C(CH3)3; reaction at 80°C in presence of azoisobutyric acid dinitrile; reaction mechanism discussed;;
参考文献
Kuivila, H. G.; Menapace, L. W.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2165 - 2167
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.2, page 52 - 57
反应条件
iodine; magnesium in tetrahydrofuran 7 h; Heating;
参考文献
Leffler, J.E.; Barbas, J.T.
Journal of the American Chemical Society, 1981 , vol. 103, # 26 p. 7768 - 7773
反应条件
diethyl ether; magnesium anschliessend Behandeln mit festem Kohlendioxid;
参考文献
Zieger, Herman; Perri, Carolyn; Bharucha, Kamal
Tetrahedron Letters, 1987 , vol. 28, # 48 p. 5989 - 5992
反应条件
(i) NaN3, HMPT, (ii) Pd-C, benzene; Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 49, p. 506 - 509
反应条件
1.1: 1-methyl-pyrrolidin-2-one / 160 - 165 °C 2.1: AlCl3, aluminium chloride / dichloromethane / 0 - 5 °C / Inert atmosphere 2.2: 0 °C / Inert atmosphere 3.1: sodium hydroxide; methanol / 2 h / 20 °C 4.1: potassium permanganate; acetic acid / water; acetone / 0 - 20 °C 5.1: hydrogenchloride; methanol / 7 h / 40 - 45 °C View Scheme
参考文献
Jubilant Organosys Limited
Patent: EP2289867 A2, 2011 ;
参考文献
Whitmore; Weisgerber; Shabica
Journal of the American Chemical Society, 1943 , vol. 65, p. 1469
