1-(2H-1-苯并吡喃-3-基)乙酮合成路线 (共 5 条)
反应条件
1,4-diaza-bicyclo[2.2.2]octane; water in chloroform T=20°C; Addition; Baylis-Hillman reaction; 168 h;
参考文献
Kaye, Perry T.; Nocanda, Xolani W.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 10 p. 1318 - 1323
反应条件
silver hexafluoroantimonate in tetrahydrofuran; 1,2-dichloro-ethane T=80°C;
参考文献
Rhee, Jong Uk; Krische, Michael J.
Organic Letters, 2005 , vol. 7, # 12 p. 2493 - 2495
反应条件
1,4-diaza-bicyclo[2.2.2]octane in water T=20°C; 2 h;
参考文献
Ravichandran
Synthetic Communications, 2001 , vol. 31, # 8 p. 1233 - 1235
反应条件
1: K2CO3 / dimethylformamide / 70 h / 20 °C 2: 93 percent / AgSbF6 / 1,2-dichloro-ethane; tetrahydrofuran / 80 °C View Scheme
参考文献
Rhee, Jong Uk; Krische, Michael J.
Organic Letters, 2005 , vol. 7, # 12 p. 2493 - 2495
反应条件
sulfuric acid 1.) ether, reflux, 6 h, 2.) ether, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Shimizu; Hayashi; Yamada; et al.
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 1 p. 217 - 222