N-亚苄基-4-甲基苯磺酰胺合成路线 (共 129 条)
反应条件
2,2-dimethylthiolane; diethylzinc in dichloromethane; toluene T=20°C; Simmons-Smith-based aziridation; 16 h;
参考文献
European Journal of Organic Chemistry, , # 2 p. 319 - 326
反应条件
ammonium chloride; zinc in dichloromethane; water T=25°C; 0.5 h;
参考文献
Tetrahedron, , vol. 65, # 7 p. 1321 - 1326
反应条件
1: iso-propylmagnesium bromide With trimethylsilyl-methylmagnesium chloride; lithium chloride; zinc(II) chloride in tetrahydrofuran; diethyl ether T=20°C; 0.75 h; Inert atmosphere; 2: N-benzylidene-4-methylbenzenesulfonamide in tetrahydrofuran; diethyl ether T=20°C; 2 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 75, # 15 p. 5008 - 5016
反应条件
ammonium chloride; zinc in dichloromethane; water T=25°C; 0.5 h;
参考文献
Tetrahedron, , vol. 65, # 7 p. 1321 - 1326
反应条件
ammonium chloride; zinc in dichloromethane; water T=25°C; 0.5 h;
参考文献
Tetrahedron, , vol. 65, # 7 p. 1321 - 1326
反应条件
diethylzinc in toluene Inert atmosphereReflux;
参考文献
Yin, Chao; Hu, Xiu-Qin; Hui, Xin-Ping; Xu, Peng-Fei
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 10 p. 1512 - 1516
反应条件
copper(l) iodide; potassium tert-butylate; diethylzinc in tetrahydrofuran; hexane; toluene T=20°C; 2 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 56, # 1 p. 57 - 59
反应条件
triethyl borane; tris-(trimethylsilyl)silane; 1,1,1-trifluoro-N-(4-oxido-2,6-bis(2,4,6-triisopropylphenyl)dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yl)methanesulfonamide; oxygen in tetrahydrofuran T=-40°C; 6 h; enantioselective reaction;
参考文献
Tetrahedron Letters, , vol. 50, # 26 p. 3345 - 3348
反应条件
in dichloromethane T=20°C; 16 h; Molecular sieve;
参考文献
Organic Letters, , vol. 14, # 1 p. 82 - 85
反应条件
hydrogenchloride; samarium in tetrahydrofuran T=20°C; Title compound not separated from byproducts;
参考文献
Liu, Xi; Liu, Yunkui; Zhang, Yongmin
Tetrahedron Letters, 2002 , vol. 43, # 38 p. 6787 - 6789