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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
51738-10-4
合成路线
（共 22 条）
110-89-4
哌啶
+
51738-10-4
→
反应条件
105072-35-3
反应条件
potassium hydroxide in tetrahydrofuran; water T=20°C; 15 h;
参考文献
Huh, Dal Ho; Jeong, Ji Sang; Lee, Hee Bong; Ryu, Hoejin; Kim, Young Gyu
Tetrahedron, 2002 , vol. 58, # 50 p. 9925 - 9932
110-89-4
哌啶
+
51738-10-4
→
反应条件
105072-35-3
反应条件
water T=20°C; 5 h;
参考文献
Huh, Dal Ho; Jeong, Ji Sang; Lee, Hee Bong; Ryu, Hoejin; Kim, Young Gyu
Tetrahedron, 2002 , vol. 58, # 50 p. 9925 - 9932
51738-10-4
→
反应条件
937-31-5
1-乙炔基-4-硝基苯
反应条件
caesium carbonate; dimethyl sulfoxide T=80°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 52, # 9 p. 992 - 994
51738-10-4
→
反应条件
926265-87-4
[4-(2-氧代-2-吡咯烷-1-基乙基)苯基]胺盐酸盐
反应条件
1: water / 20 °C 2: 10 palladium on activated charcoal; hydrogen / methanol View Scheme
参考文献
Wang, Li; Yang, Fenyan; Yang, Xiaochun; Guan, Xianghong; Hu, Chunqi; Liu, Tao; He, Qiaojun; Yang, Bo; Hu, Yongzhou
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 1 p. 285 - 296
51738-10-4
→
反应条件
210158-20-6
反应条件
1: water / 20 °C 2: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / Reflux View Scheme
参考文献
Wang, Li; Yang, Fenyan; Yang, Xiaochun; Guan, Xianghong; Hu, Chunqi; Liu, Tao; He, Qiaojun; Yang, Bo; Hu, Yongzhou
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 1 p. 285 - 296
504-29-0
2-氨基吡啶
+
51738-10-4
→
反应条件
3323-26-0
反应条件
potassium fluoride in N,N-dimethyl-formamide T=20 - 130°C; 12.1667 h; Inert atmosphere; regioselective reaction;
参考文献
Liu, Guoping; Cong, Xuefeng; He, Jiaheng; Luo, Shunzhong; Wu, Di; Lan, Jingbo
Journal of Chemical Research, 2012 , vol. 36, # 12 p. 687 - 690
51738-10-4
→
反应条件
104-03-0
对硝基苯乙酸
反应条件
1: 97 percent / KOH / tetrahydrofuran; H2O / 8 h / 20 °C 2: 77 percent / H2O / 20 °C 3: 91 percent / aq. HCl / dioxane / 12 h / Heating View Scheme
参考文献
Huh, Dal Ho; Jeong, Ji Sang; Lee, Hee Bong; Ryu, Hoejin; Kim, Young Gyu
Tetrahedron, 2002 , vol. 58, # 50 p. 9925 - 9932
51738-10-4
→
反应条件
168897-19-6
4-(2-(1-吡咯烷)乙基)硝基苯
反应条件
1: water / 20 °C 2: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / Reflux View Scheme
参考文献
Wang, Li; Yang, Fenyan; Yang, Xiaochun; Guan, Xianghong; Hu, Chunqi; Liu, Tao; He, Qiaojun; Yang, Bo; Hu, Yongzhou
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 1 p. 285 - 296
51738-10-4
→
反应条件
168897-20-9
反应条件
1: water / 20 °C 2: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / Reflux 3: 10 palladium on activated charcoal; hydrogen / methanol View Scheme
参考文献
Wang, Li; Yang, Fenyan; Yang, Xiaochun; Guan, Xianghong; Hu, Chunqi; Liu, Tao; He, Qiaojun; Yang, Bo; Hu, Yongzhou
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 1 p. 285 - 296
51738-10-4
→
反应条件
262368-47-8
反应条件
1: water / 20 °C 2: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / Reflux 3: 10 palladium on activated charcoal; hydrogen / methanol View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 46, # 1 p. 285 - 296
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