1: N-(tert-butyloxycarbonyl)pyrrole With lithium diisopropyl amide in tetrahydrofuran; hexane T=-71°C; 6 h; 2: dimethyl-dichlorosilane in tetrahydrofuran; hexane T=-71 - 20°C; 10 h; 3: With sodium hydrogencarbonate in tetrahydrofuran; hexane; water cooling; Further stages.;
参考文献
Denmark, Scott E.; Baird, John D.; Regens, Christopher S.
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1440 - 1455
Gregersen, Anette; Pedersen, Christian Marcus; Jensen, Henrik Helligso; Bols, Mikael
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 8 p. 1514 - 1519
1: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2 h; 2: With boric acid trimethyl ester in tetrahydrofuran; hexane T=20°C; Further stages.;
参考文献
Haynes, Stuart W.; Sydor, Paulina K.; Stanley, Anna E.; Song, Lijiang; Challis, Gregory L.
Chemical Communications, 2008 , # 16 p. 1865 - 1867
