tetrahydrofuran in tetrahydrofuran
4°C (2 days); various product ratios for various conditions; removal of solvent, addn. of hexane;
参考文献
Markevich, I. N.; Sharaev, O. K.; Tinyakova, E. I.; Dolgoplosk, B. A.
Doklady Chemistry, 1983 , vol. 268, p. 43 - 46
Dokl. Akad. Nauk SSSR Ser. Khim., 1983 , vol. 268, # 4 p. 892 - 896
1: diphenyl-phenyl carbinol With tetrafluoroboric acid in diethyl ether; water
T=20°C; 2 h; Molecular sieveInert atmosphere;
2: With hydrogen in diethyl ether; water
T=-70°C; 0.5 h;
3: It-Bu2 in diethyl ether; water
T=-70 - 20°C; 2.5 h;
参考文献
Runyon, Jason W.; Steinhof, Oliver; Dias, H. V. Rasika; Calabrese, Joseph C.; Marshall, William J.; Arduengo, Anthony J.
Australian Journal of Chemistry, 2011 , vol. 64, # 8 p. 1165 - 1172
