反应条件
in acetonitrile
byproducts: triethanolamine hydrobromide; under dry N2; mixt. boiled (81°C, 3 h); hot soln. decanted vac.-evapd. (20-100 mm, 30-35°C) until crystn. set in; ether added; solid 1-(triphenylmethyl)germatrane isolated; ppt. of chlorogermatrane obtained by evapn. of filtrate (40-50°C, 40mm); Ph3CH isolated from soln.; PMR;
参考文献
Gar, T. K.; Khromova, N. Yu.; Tandura, S. N.; Mironov, V. F.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 1619 - 1626
Zhurnal Obshchei Khimii, 1983 , vol. 53, p. 1800 - 1807