2,5-二乙基-3,4-二苯基环戊二酮合成路线 (共 5 条)
反应条件
sulfuric acid; acetic anhydride
参考文献
Allen; VanAllan
Journal of the American Chemical Society, 1950 , vol. 72, p. 5165
反应条件
1: 59 percent Spectr. / benzene / 8 h / 80 °C 2: various solvent(s) / 80 °C View Scheme
参考文献
Jikyo, Tamaki; Eto, Masashi; Harano, Kazunobu
Tetrahedron, 1999 , vol. 55, # 19 p. 6051 - 6066
反应条件
potassium hydroxide; sulfuric acid 1) ethanol, reflux, 2 h, 2) acetic anhydride, reflux; Multistep reaction;
参考文献
Samanta, S. R.; Mukherjee, A. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 26 - 29
反应条件
in chloroform-d1 T=-30°C; Equilibrium constantThermodynamic data;
参考文献
Weiss, Hilton M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 4 p. 439 - 443
反应条件
in xylene
6 h; Heating;
参考文献
Bandyopadhyay, T. K.; Bhattacharya, A. J.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 6 p. 439 - 442