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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
对碘苯甲酸乙酯
合成路线
（共 291 条）
51934-41-9
对碘苯甲酸乙酯
+
4294-57-9
对甲苯基溴化镁
→
反应条件
613-33-2
4,4'-二甲基联苯
+
106508-97-8
4'-甲基联苯-4-羧酸乙酯
反应条件
C80H88Cl2N6NiP2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=25°C; Kumada coupling reaction; 4 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Chemistry - A European Journal, 2010 , vol. 16, # 34 p. 10332 - 10336
696-62-8
4-碘苯甲醚
+
51934-41-9
对碘苯甲酸乙酯
→
反应条件
47230-38-6
联苯-4,4-草酸二乙酯
+
2132-80-1
+
732-80-9
+
100-66-3
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
51934-41-9
对碘苯甲酸乙酯
+
637-44-5
→
反应条件
886-66-8
+
63164-96-5
反应条件
1: 3-phenyl-2-propynoic acid With silver(l) oxide in dimethyl sulfoxide Inert atmosphere; 2: 4-iodobenzoic acid ethyl ester With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenylphosphine in dimethyl sulfoxide T=140°C; Sonogashira coupling; 3 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 17 p. 2827 - 2832
51934-41-9
对碘苯甲酸乙酯
+
637-44-5
+
471-25-0
→
反应条件
反应条件
1: 4-iodobenzoic acid ethyl ester; acetylenecarboxylic acid With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in N,N-dimethyl-formamide T=20°C; Sonogashira coupling; 6 h; Inert atmosphereSealed tube; 2: 3-phenyl-2-propynoic acid With triethylamine; silver carbonate in N,N-dimethyl-formamide T=130°C; 20 h; Inert atmosphereSealed tube;
参考文献
Journal of Organic Chemistry, , vol. 76, # 7 p. 2214 - 2219
→
反应条件
321903-29-1
反应条件
potassium carbonate; trifuran-2-yl-phosphane; palladium dichloride in dimethyl sulfoxide T=35°C; 21 h;
参考文献
Nakao, Yoshiaki; Hiyama, Tamejiro
Patent: US2009/69577 A1, 2009 ;
Location in patent: Page/Page column 20 ;
51934-41-9
对碘苯甲酸乙酯
+
106-95-6
→
反应条件
19819-94-4
反应条件
1: 4-iodobenzoic acid ethyl ester With diethylzinc in hexane; N,N-dimethyl-formamide T=20°C; 5 h; 2: allyl bromide in hexane; N,N-dimethyl-formamide T=20°C; 20 h; Further stages.;
参考文献
Ueno, Masahiro; Wheatley, Andrew E. H.; Kondo, Yoshinori
Chemical Communications, 2006 , # 33 p. 3549 - 3550
556-56-9
+
51934-41-9
对碘苯甲酸乙酯
→
反应条件
19819-94-4
反应条件
indium; triphenylphosphine; lithium chloride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in N,N-dimethyl-formamide T=100°C; 2 h;
参考文献
Lee, Kooyeon; Kim, Hyunseok; Mo, Juntae; Lee, Phil Ho
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2147 - 2157
591-87-7
+
51934-41-9
对碘苯甲酸乙酯
→
反应条件
19819-94-4
+
47230-38-6
联苯-4,4-草酸二乙酯
反应条件
1: ethylene,methyl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 2: 4-iodobenzoic acid ethyl ester in N,N-dimethyl-formamide T=100°C;
参考文献
Seomoon, Dong; Lee, Kooyeon; Kim, Hyunseok; Lee, Phil Ho
Chemistry - A European Journal, 2007 , vol. 13, # 18 p. 5197 - 5206
591-87-7
+
51934-41-9
对碘苯甲酸乙酯
→
反应条件
19819-94-4
+
869061-80-3
反应条件
dimethyl(n-butyl)amine; tetrabutyl-ammonium chloride; palladium on activated charcoal in water; N,N-dimethyl-formamide T=180°C; 1 h;
参考文献
Mariampillai, Brian; Herse, Christelle; Laufens, Mark
Organic Letters, 2005 , vol. 7, # 21 p. 4745 - 4747
51934-41-9
对碘苯甲酸乙酯
+
107-05-1
→
反应条件
19819-94-4
反应条件
1: 4-iodobenzoic acid ethyl ester With chloro-trimethyl-silane; zinc in diethylene glycol dimethyl ether T=100°C; 24 h; 2: 3-chloroprop-1-ene With bis(dibenzylideneacetone)-palladium(0) in diethylene glycol dimethyl ether T=0°C; 0.166667 h;
参考文献
Ikegami, Ryo; Koresawa, Akiko; Shibata, Takanori; Takagi, Kentaro
Journal of Organic Chemistry, 2003 , vol. 68, # 6 p. 2195 - 2199
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