hydrogenchloride in dichloromethane Ambient temperature;

1: 100 percent / N-bromosuccinimide / CCl4 / 15 °C / Irradiation 2: 61 percent / CH2Cl2 / Ambient temperature 3: 85 percent / HCl (gas) / CH2Cl2 / Ambient temperature View Scheme

1: 1) 20percent aq. solution of Cs2CO3 / 1) MeOH, water, pH 7.0, 2) DMF, 5 h 2: 100 percent / N-bromosuccinimide / CCl4 / 15 °C / Irradiation 3: 61 percent / CH2Cl2 / Ambient temperature 4: 85 percent / HCl (gas) / CH2Cl2 / Ambient temperature View Scheme

1: 61 percent / CH2Cl2 / Ambient temperature 2: 85 percent / HCl (gas) / CH2Cl2 / Ambient temperature View Scheme

暂无反应条件数据

toluene-4-sulfonic acid in diethyl ether

O-(diphenyl-phosphinyl)hydroxylamine; sodium hydride 1.) THF, room temp., 1 h, 2.) THF, -78 deg C, 2 h, room temp.; Yield given. Multistep reaction;