(3-苯基-2H-氮杂环丙烯-2-基)甲醇合成路线 （共 5 条）
参考文献
Sakai; Kawabata; Kishimoto; Ema; Utaka
Journal of Organic Chemistry, 1997 , vol. 62, # 15 p. 4906 - 4907
反应条件
1: 1) NaN3, 2) NaOH / 1) DMSO, 2) DMSO
2: 88 percent / toluene / 80 °C
View Scheme
参考文献
Sakai; Kawabata; Kishimoto; Ema; Utaka
Journal of Organic Chemistry, 1997 , vol. 62, # 15 p. 4906 - 4907
反应条件
1: 87 percent / Br2 / CH2Cl2
2: 1) NaN3, 2) NaOH / 1) DMSO, 2) DMSO
3: 88 percent / toluene / 80 °C
View Scheme
参考文献
Sakai; Kawabata; Kishimoto; Ema; Utaka
Journal of Organic Chemistry, 1997 , vol. 62, # 15 p. 4906 - 4907
反应条件
1.1: polymer-NMe3(+) I(N3)2(-) / dichloromethane / 24 h / |Darkness
1.2: 4 h / 20 °C
2.1: |Flow reactor; |UV-irradiation
View Scheme
参考文献
Cludius-Brandt, Stephan; Kupracz, Lukas; Kirschning, Andreas
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1745 - 1750
反应条件
Flow reactorUV-irradiation; Temperature;
参考文献
Cludius-Brandt, Stephan; Kupracz, Lukas; Kirschning, Andreas
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1745 - 1750
