1,2-二(4-氯苯基)乙烷合成路线 (共 79 条)
反应条件
copper(l) iodide; chloro-trimethyl-silane; iodine; lanthanum in acetonitrile
T=82°C; 1 h;
参考文献
Nishino, Toshiki; Nishiyama, Yutaka; Sonoda, Noboru
Tetrahedron Letters, 2002 , vol. 43, # 20 p. 3689 - 3691
反应条件
1: With NiCl2((PPh3)P)2
0.5 h;
2: in tetrahydrofuran
参考文献
REGENTS OF THE UNIVERSITY OF MINNESOTA; VINCE, Robert; VARTAK, Ashish P.
Patent: WO2012/128965 A2, 2012 ;
Location in patent: Page/Page column 15-16 ;
反应条件
carbon monoxide; copper; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
P=760 Torr; -78 deg C, 2h; room temp., 1 h; 60 deg C, 6 h; Further byproducts given;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yamada, Yoshimi; Yoshida, Zen-ichi
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3869 - 3872
反应条件
copper; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
P=760 Torr; -78 deg C, 2h; room temp., 1 h; 60 deg C, 6 h; Further byproducts given;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yamada, Yoshimi; Yoshida, Zen-ichi
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3869 - 3872
反应条件
pyridine in dichloromethane
T=0°C; 5.33333 h; Irradiation;
参考文献
Gupta, B. D.; Das, Indira; Dixit, Vandana
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, 1993 , vol. 32, # 9 p. 762 - 766
反应条件
T=600°C; P=20 Torr; 0.0333333 h;
参考文献
Higuchi, Hiroyuki; Otsubo, Tetsuo; Ogura, Fumio; Yamaguchi, Hachiro; Sakata, Yoshiteru; Misumi, Soichi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 1 p. 182 - 187
反应条件
pyridine; 4-chloro-benzenesulfonyl chloride in dichloromethane
T=0°C; 2 h; Irradiation;
参考文献
Gupta, B. Dass; Roy, Maheswar; Roy, Sujit; Kumar, Manoj; Das, Indira
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 4 p. 537 - 543
反应条件
pyridine in dichloromethane
T=0°C; 2 h; Irradiation;
参考文献
Gupta, B. Dass; Roy, Maheswar; Roy, Sujit; Kumar, Manoj; Das, Indira
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 4 p. 537 - 543
反应条件
[RuCl2(SIMes)(P(p-ClPh)3)(3-phenylinden-1-ylidene)] in dichloromethane
T=20°C; 3 h; Inert atmosphere; stereoselective reaction;
参考文献
Broggi, Julie; Urbina-Blanco, Cesar A.; Clavier, Herve; Leitgeb, Anita; Slugovc, Christian; Slawin, Alexandra M. Z.; Nolan, Steven P.
Chemistry - A European Journal, 2010 , vol. 16, # 30 p. 9215 - 9225
参考文献
Higuchi, Hiroyuki; Sakata, Yoshiteru; Misumi, Soichi; Otsubo, Tetsuo; Ogura, Fumio; Yamaguchi, Hachiro
Chemistry Letters, 1981 , p. 627 - 630