1,2-二(4-氯苯基)乙烷合成路线 （共 79 条）
反应条件
in further solvent(s)
pyrolysis in p-chlorotoluene under dry and deoxygenated N2 (stirring; 140°C, 9 h); GLC anal. of org. products;
参考文献
Nomura, Ryoki; Miyazaki, Shin-Ichiro; Matsuda, Haruo
Organometallics, 1992 , vol. 11, p. 2 - 4
反应条件
T=600°C; 0.0833333 h;
参考文献
Otsubo, Tetsuo; Ogura, Fumio; Yamaguchi, Hachiro
Synthetic Communications, 1980 , vol. 10, # 8 p. 595 - 602
反应条件
copper; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
room temp., 5 h; 60 deg C, 18 h;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yamada, Yoshimi; Yoshida, Zen-ichi
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3869 - 3872
反应条件
copper; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
60 deg C, 9 h;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yamada, Yoshimi; Yoshida, Zen-ichi
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3869 - 3872
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tert-butyl alcohol
3 h; Heating;
参考文献
Marquet, Jorge; Moreno-Manas, Marcial; Pacheco, Pedro; Prat, Maria; Katritzky, Alan R.; Brycki, Bogumil
Tetrahedron, 1990 , vol. 46, # 15 p. 5333 - 5346
反应条件
trimethylhexadecylammonium chloride in water
Irradiationcage effect under variety conditions; Quantum yield;
参考文献
Turro, Nicholas J.; Weed, Gregory C.
Journal of the American Chemical Society, 1983 , vol. 105, # 7 p. 1861 - 1868
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tert-butyl alcohol
3 h; Heating;
参考文献
Marquet, Jorge; Moreno-Manas, Marcial; Pacheco, Pedro; Prat, Maria; Katritzky, Alan R.; Brycki, Bogumil
Tetrahedron, 1990 , vol. 46, # 15 p. 5333 - 5346
反应条件
1,3,5-trimethyl-benzene; naphthalenyl-1-carbonitrile in acetonitrile
T=20°C; Irradiationother 4,4'-disubstituted dibenzyl ketones; var. donor-acceptor systems; Product distribution;
参考文献
Ishiguro, Katsuya; Nakano, Tomoharu; Shibata, Hiroki; Sawaki, Yasuhiko
Journal of the American Chemical Society, 1996 , vol. 118, # 31 p. 7255 - 7264
反应条件
1: 86 percent / NaBH4 / benzene / 1 h / Ambient temperature
2: 68 percent / 0.08 h / 600 °C
View Scheme
参考文献
Otsubo, Tetsuo; Ogura, Fumio; Yamaguchi, Hachiro
Synthetic Communications, 1980 , vol. 10, # 8 p. 595 - 602
反应条件
1: KI
2: Zn
3: H2 / Raney-Ni
View Scheme
参考文献
Weis,C.D.
Helvetica Chimica Acta, 1966 , vol. 49, p. 234 - 243
