暂无反应条件数据

in diethyl ether T=20°C; Inert atmosphere;

(i) , (ii) /BRN= 1420755/, aq.NaOH, (iii) I2, (heating); Multistep reaction;

in diethyl ether T=20°C; Inert atmosphere;

in tetrahydrofuran byproducts: NaCl; under Ar, to stirred soln. of Cp2TiCl2 in THF added portionwise within 1 h suspn. of NaSC6H4NH2 in THF, stirred at room temp. for 2 h; filtered, concd. in vac., pentane added, allowed to stand at room temp.for 20 h, filtered, concd., ppt. sepd., washed with toluene, dried in vac.; elem. anal.;

in ethanol Reflux;

暂无反应条件数据

2: (i) aq. HCl, NaNO2, (ii) /BRN= 774278/, NaOAc View Scheme