1-甲基-4,9-二氢-3H-吡啶并[3,4-b]吲哚合成路线 （共 19 条）
反应条件
1: 11 percent / toluene / 1.5 h / Heating
2: 0.2 g / HCl(g) / CHCl3 / 24 h / 25 °C
View Scheme
参考文献
Bobowski; Shavel Jr.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 6 p. 1679 - 1688
反应条件
hydrogenchloride in chloroform
T=25°C; 0.0333333 h;
参考文献
Bobowski, George
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 267 - 272
反应条件
hydrogenchloride in chloroform
T=25°C; 24 h;
参考文献
Bobowski; Shavel Jr.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 6 p. 1679 - 1688
反应条件
1: 82 percent / methanol; H2O / 12 h
2: 42 percent / H2O; methanol / 6 h / 25 °C / +0.8V/32mA; anode: graphite felt, cathode: Pt, electrolyte: KH2PO4/K2HPO4
View Scheme
参考文献
Bobbitt, James M.; Willis, John P.
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1978 - 1984
反应条件
trichlorophosphate in acetonitrile
参考文献
Frost, Jonathan R.; Gaudilliere, Bernard R. P.; Wick, Alexander E.
Journal of the Chemical Society, Chemical Communications, 1985 , # 13 p. 895 - 897
反应条件
water; silver(l) oxide
参考文献
Spenser
Canadian Journal of Chemistry, 1959 , vol. 37, p. 1851,1856
反应条件
1: zinc chloride
3: P2O5; xylene
View Scheme
参考文献
Spaeth; Lederer
Chemische Berichte, 1930 , vol. 63, p. 120,123
反应条件
formic acid; (S,S)-TsDPEN-Ru(II); triethylamine in N,N-dimethyl-formamide
T=20°C; 12 h; optical yield given as percent eeenantioselective reaction;
参考文献
Da Silva, Wender A.; Rodrigues Jr., Manoel T.; Shankaraiah; Ferreira, Renan B.; Andrade, Carlos Kleber Z.; Pilli, Ronaldo A.; Santos, Leonardo S.
Organic Letters, 2009 , vol. 11, # 15 p. 3238 - 3241
反应条件
sodium trislt;(S)-N-benzyloxycarbonylprolyloxygt;hydroborate in dichloromethane
22 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yamada, Koichiro; Takeda, Mikio; Iwakuma, Takeo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 2 p. 265 - 270
